524220
2,5-Diethoxyaniline
97%
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About This Item
Linear Formula:
(C2H5O)2C6H3NH2
CAS Number:
Molecular Weight:
181.23
NACRES:
NA.22
PubChem Substance ID:
UNSPSC Code:
12352100
EC Number:
202-369-5
MDL number:
Assay:
97%
Form:
solid
InChI key
XPKFTIYOZUJAGA-UHFFFAOYSA-N
InChI
1S/C10H15NO2/c1-3-12-8-5-6-10(13-4-2)9(11)7-8/h5-7H,3-4,11H2,1-2H3
SMILES string
CCOc1ccc(OCC)c(N)c1
assay
97%
form
solid
mp
85-88 °C (lit.)
General description
2,5-Diethoxyaniline is a primary aromatic amine. It can be obtained from 2,5-diethoxynitrobenzene, via reduction with Me3SiSNa. Phthalimidomethyl derivatives formed by the condensation of 2,5-Diethoxyaniline and phthalimidomethyl could be used for the characterization of amines.
Application
2,5-Diethoxyaniline may be used to synthesize 4-chloro-2′,5′-diethoxy-2-nitrodiphenylamine and methyl 2-chloro-3-(2,5-diethoxyphenyl)propionate.
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
Storage Class
11 - Combustible Solids
wgk
WGK 1
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
dust mask type N95 (US), Eyeshields, Gloves
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Direct ring closure through the nitro group. Isomer formation in the synthesis of unsymmetrical phenazines, and some general observations on the phenazine syntheses.
Vivian DL ,et al.
The Journal of Organic Chemistry, 16(1), 1-7 (1951)
Antiulcer activity of 5-benzylthiazolidine-2, 4-dione derivatives.
Sohda T, et al.
Chemical & Pharmaceutical Bulletin, 31(2, 560-569 (1983)
Identification of Amines. II. Phthalimidomethyl Derivatives of Primary and Secondary Amines1.
Heine HW, et al.
Journal of the American Chemical Society, 78(3), 672-674 (1956)
Reduction of aromatic nitro compounds to aromatic amines by sodium trimethylsilanethiolate.
Hwu JR, et al.
The Journal of Organic Chemistry, 57(19), 5254-5255 (1992)
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