528595
2,6-Diethoxybenzoic acid
97%
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About This Item
Linear Formula:
(C2H5O)2C6H3CO2H
CAS Number:
Molecular Weight:
210.23
NACRES:
NA.22
PubChem Substance ID:
UNSPSC Code:
12352100
MDL number:
InChI
1S/C11H14O4/c1-3-14-8-6-5-7-9(15-4-2)10(8)11(12)13/h5-7H,3-4H2,1-2H3,(H,12,13)
SMILES string
CCOc1cccc(OCC)c1C(O)=O
InChI key
XUIVSLVJEQVKLB-UHFFFAOYSA-N
assay
97%
form
solid
mp
131-135 °C (lit.)
General description
2,6-Diethoxybenzoic acid undergoes catalytic hydrodecarboxylation in the presence of toluene/D2O to afford 2-d-1,3-diethoxybenzene.
Storage Class
13 - Non Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Eyeshields, Gloves, type N95 (US)
Regulatory Information
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Jing Zhang et al.
Journal of the American Chemical Society, 135(46), 17270-17273 (2013-11-01)
Through-space metal/hydrogen shift is an important strategy for transition-metal-catalyzed C-H bond activation. Here we describe the synthesis and characterization of a Rh(I) 2,6-dimethoxybenzoate complex that underwent stoichiometric rearrangement via a highly unusual 1,3-rhodium migration. This aryl-to-aryl 1,3-Rh/H shift was also
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