714836
Iodine monochloride solution
1 M in acetic acid
Synonym(s):
Chloroiodide solution, Wijs solution
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About This Item
Linear Formula:
ICl
CAS Number:
Molecular Weight:
162.36
UNSPSC Code:
12352101
NACRES:
NA.22
PubChem Substance ID:
MDL number:
Beilstein/REAXYS Number:
3587194
Form:
solution
InChI key
QZRGKCOWNLSUDK-UHFFFAOYSA-N
SMILES string
ClI
InChI
1S/ClI/c1-2
form
solution
concentration
1 M in acetic acid
density
1.143 g/mL at 25 °C
Quality Level
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General description
Iodine monochloride is an inorganic reagent used in the iodination and chloroiodination of aromatic and unsaturated compounds, respectively. It is also used to cleave carbon-metal bonds.
Application
Iodine monochloride can be used:
- As a reagent in the preparation of α-iodo β-ketosulfones from β-ketosulfones.
- In the synthesis of 3-(4-bromo-2-methylphenyl)-4-iodosydnone, which is further used to prepare substituted pyrazoles.
signalword
Danger
hcodes
Hazard Classifications
Eye Dam. 1 - Flam. Liq. 3 - Skin Corr. 1B
Storage Class
3 - Flammable liquids
wgk
WGK 3
flash_point_f
105.1 °F
flash_point_c
40.6 °C
Regulatory Information
危险化学品
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Synthesis of α-iodo β-ketosulfones and α-iodo methylsulfones using iodine monochloride
Suryakiran N, et al.
Tetrahedron Letters, 47(26), 4319-4323 (2006)
Iodine monochloride
e-EROS Encyclopedia of Reagents for Organic Synthesis. (2013)
Steric effects on the sydnones reactivity. New sydnones and pyrazoles
Dumitracscu F, et al.
ARKIVOC (Gainesville, FL, United States), 2(26), 80-86 (2002)
Iodine monochloride (IC1) iodination techniques.
M A Contreras et al.
Methods in enzymology, 92, 277-292 (1983-01-01)
Cell surface labeling by iodine monochloride.
E J Victoria et al.
The International journal of biochemistry, 13(9), 1011-1017 (1981-01-01)
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