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Merck
CN

93197

Sigma-Aldrich

Poly-L-leucine-1,3-diaminopropane

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MDL number:
UNSPSC Code:
12352200
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form

powder

application(s)

peptide synthesis

Application

Catalyst employed for the enantioselective epoxidation of enones to epoxy ketones (Juliá-Colonna epoxidation) in heterogeneous phase. Green epoxidation catalyst of choice according to Glaxo-Smith-Kline's reagent guide.

Novel conditions for the Juliá–Colonna epoxidation reaction providing efficient access to chiral, nonracemic epoxides

Other Notes

Catalyst employed for the enantioselective epoxidation of enones to epoxy ketones (Juliá-Colonna epoxidation) in heterogeneous phase

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Warning

Hazard Statements

Precautionary Statements

Hazard Classifications

Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3

Storage Class Code

13 - Non Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

Regulatory Information

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R W Flood et al.
Organic letters, 3(5), 683-686 (2001-03-22)
[reaction: see text]. Polyethylene glycol (PEG)-bound poly-L-leucine acts as a THF-soluble catalyst for the Juliá-Colonna asymmetric epoxidation of enones. Excellent enantioselectivities may be obtained even with short chain length polyleucine. FT-IR investigations have determined that the catalytically active polyleucine components
C. Lauret
Tetrahedron Asymmetry, 12, 2359-2359 (2001)

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