T60402
Triethyl orthoacetate
97%
Synonym(s):
1,1,1-Triethoxyethane
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About This Item
Linear Formula:
CH3C(OC2H5)3
CAS Number:
Molecular Weight:
162.23
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
EC Number:
201-112-4
Beilstein/REAXYS Number:
506201
MDL number:
Assay:
97%
InChI key
NDQXKKFRNOPRDW-UHFFFAOYSA-N
InChI
1S/C8H18O3/c1-5-9-8(4,10-6-2)11-7-3/h5-7H2,1-4H3
SMILES string
CCOC(C)(OCC)OCC
assay
97%
Quality Level
bp
142 °C (lit.)
density
0.885 g/mL at 25 °C (lit.)
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Application
Triethyl orthoacetate can be used for the synthesis of:
- Ordered mesoporous carbons for catalysis, electrochemistry and hydrogen storage applications.
- Esters of phosphonic acids, carboxylic acids and phosphinic acids.
- Ethyl alk-4-enoates by Johnson–Claisen rearrangement reaction.
- Benzoxazoles, benzimidazoles and oxazolo[4,5-b]pyridines.
- Quinazolin-4(3H)-one derivatives.
signalword
Warning
hcodes
Hazard Classifications
Flam. Liq. 3
Storage Class
3 - Flammable liquids
flash_point_f
102.2 °F - Non-equilibrium method
flash_point_c
39 °C - Non-equilibrium method
ppe
Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
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Silica sulfuric acid catalyzed synthesis of benzoxazoles, benzimidazoles and oxazolo [4, 5-b] pyridines under heterogeneous and solvent-free conditions
Mohammadpoor-Baltork I, et al.
Journal of the Iranian Chemical Society, 5(1), S65-S70 (2008)
Synthesis of ordered mesoporous carbons with channel structure from an organic-organic nanocomposite
Tanaka S, et al.
Chemical Communications (Cambridge, England), 16, 2125-2127 (2005)
Treatment of Baylis-Hillman adducts with triethyl orthoacetate in the presence of heterogeneous catalysts: a method for the stereoselective synthesis of two different types of trisubstituted alkenes
Das B, et al.
Tetrahedron Letters, 47(43), 7619-7623 (2006)
Efficient esterification of carboxylic acids and phosphonic acids with trialkyl orthoacetate in ionic liquid
Yoshino T, et al.
Tetrahedron, 62(6), 1309-1317 (2006)
A new approach to the facile synthesis of mono-and disubstituted quinazolin-4 (3H)-ones under solvent-free conditions.
Salehi P, et al.
Tetrahedron Letters, 46(41), 7051-7053 (2005)
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