92078
2,4,6-Triisopropylbenzenesulfonohydrazide
technical, ≥90% (HPLC)
Synonym(s):
TPSH, Trisylhydrazide
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About This Item
Linear Formula:
[(CH3)2CH]3C6H2SO2NHNH2
CAS Number:
Molecular Weight:
298.44
EC Number:
254-282-7
UNSPSC Code:
12352100
PubChem Substance ID:
Beilstein/REAXYS Number:
2145001
MDL number:
grade
technical
assay
≥90% (HPLC)
mp
110-112 °C (dec.) (lit.)
storage temp.
−20°C
SMILES string
CC(C)c1cc(C(C)C)c(c(c1)C(C)C)S(=O)(=O)NN
InChI
1S/C15H26N2O2S/c1-9(2)12-7-13(10(3)4)15(20(18,19)17-16)14(8-12)11(5)6/h7-11,17H,16H2,1-6H3
InChI key
UGRVYFQFDZRNMQ-UHFFFAOYSA-N
Other Notes
Convenient source of diimide; For the preparation of vinyllithium compounds from ketones (Sharpio reaction); For the synthesis of homologated nitriles from aldehydes and ketones; For the preparation of aryldiazoalkanes
Storage Class
13 - Non Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Eyeshields, Gloves, type N95 (US)
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R.M. Adlington et al.
Accounts of Chemical Research, 16, 55-55 (1983)
J.J. Jiricny et al.
Journal of the Chemical Society. Perkin Transactions 1, 1487-1487 (1980)
C.C. Dudman et al.
Synthesis, 419-419 (1982)
N.J. Cusack et al.
Tetrahedron, 32, 2157-2157 (1976)
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