13081-U
Glass Packed GC Column (fits Agilent, Configuration "A")
phase 10% FFAP + 1% H3PO4, matrix 100/120 Chromosorb W AW support, L × O.D. × I.D. 6.0 ft (1.8 m) × 1/4 in. × 2.0 mm
material
glass column
manufacturer/tradename
Agilent
parameter
60-225 °C temperature (isothermal or programmed)
technique(s)
gas chromatography (GC): suitable
L × O.D. × I.D.
6.0 ft (1.8 m) × 1/4 in. × 2.0 mm
matrix
100/120 Chromosorb W AW support
matrix active group
10% FFAP + 1% H3PO4 phase
column type
packed GC
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General description
In a packed column, the carrier gas percolates through the porous bed and separation is achieved by moving the solutes apart. Packed columns are made up of two main materials; stainless steel and Pyrex glass. Pyrex glass columns are shaped as desired by coiling at about 700°C. Glass column are in some cases treated with silanizing reagent to eliminate the surface hydroxyl groups which becomes catalytically active and produce asymmetric peaks. Chromosorb W, a fragile white solid prepared by heating the diatomaceous earth with a flux. The resulting fine structure is cemented over glass which results in large and irregular pores. Chromosorb W provides a relatively inert surface and is suitable for polar compounds. Chromosorb W needs to be acid washed (AW) followed by silanized to make it less active and more inert.
Use a glass column for applications where high inertness is required, such as for the analysis of active analytes. All glass columns undergo a proprietary high temperature silanization to ensure inertness. This column fits Agilent 5880, 5890, 6890. 7820, and 7890 (configuration A, on-column injection, all detectors except TCD).
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Satinder Ahuja
Chromatography and Separation Science, 137-138 (2003)
Ian A. Fowlis
Gas Chromatography, 27-27 (2008)
Raymond P. W. Scott
Introduction to Analytical Gas Chromatography (1997)
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