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21284-U

Supelco

GC Stationary Phase

phase SP®-2100, bottle of 10 g

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NACRES:
SB.54

Agency

meets requirements for USP G1

Quality Level

packaging

bottle of 10 g

parameter

0-350 °C temp. range

technique(s)

gas chromatography (GC): suitable

matrix active group

SP®-2100 phase

solubility

chloroform: soluble

column type

packed GC

General description

GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients. The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation, peak tailing are a few parameters that should be considered in order to choose a stationary phase. SP-2100 is a methyl silicone fluid suitable as stationary phase.
Synthesized specifically to be purer, of narrow molecular weight range, and without trace catalysts or impurities for use as a GC stationary phase.

Application

SP-2100 fused silica column deactivated with Carbowax 20M is suitable for determining optimal conditions for the analysis of fatty and resin acids in wood resin.

Legal Information

SP is a registered trademark of Sigma-Aldrich Co. LLC

Storage Class Code

10 - Combustible liquids

WGK

WGK 1

Flash Point(F)

214.0 °F - closed cup

Flash Point(C)

101.1 °C - closed cup

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

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Operating variables in the analysis of tall oil acids by capillary gas chromatography.
Dorris, G. M.
Journal of the American Oil Chemists' Society, 59, 494-500 (1982)
Stanley Blackburn
Peptides, 286-286 (1986)
James P. Lodge, Jr.
Methods of Air Sampling and Analysis, 98-98 (1988)
David B. Troy, Paul Beringer
Remington: The Science and Practice of Pharmacy, 605-605 (2006)

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