24028
SPB®-1 Capillary GC Column
L × I.D. 30 m × 0.25 mm, df 0.25 μm
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About This Item
UNSPSC Code:
41115710
eCl@ss:
32119290
material
fused silica
Quality Level
Agency
meets requirements for USP G1, G2, and G9
parameter
-60-320 °C temperature (isothermal or programmed)
Beta value
250
df
0.25 μm
technique(s)
gas chromatography (GC): suitable
L × I.D.
30 m × 0.25 mm
matrix active group
Bonded; poly(dimethyl siloxane) phase
column type
capillary non-polar
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General description
Application: This column is often used for traditional general purpose applications, where a non-polar column is required. Analytes will be separated primarily according to boiling point.
USP Code: This column meets USP G1, G2, and G9 requirements.
Phase:
USP Code: This column meets USP G1, G2, and G9 requirements.
Phase:
- Bonded
- Poly(dimethyl siloxane)
- ≤0.32 mm I.D., <2 μm: -60 °C to 320 °C (isothermal or programmed)
- ≤0.32 mm I.D., ≥2 μm: -60 °C to 300 °C (isothermal or programmed)
- ≥0.53 mm I.D., <2 μm: -60 °C to 300 °C (isothermal) or 320 °C (programmed)
- ≥0.53 mm I.D., ≥2 μm: -60 °C to 260 °C (isothermal) or 280 °C (programmed)
Application
SPB®-1 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection.
Other Notes
We offer a variety of chromatography accessories including analytical syringes
Legal Information
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany
Storage Class Code
10 - Combustible liquids
WGK
WGK 1
Flash Point(F)
214.0 °F - closed cup
Flash Point(C)
101.1 °C - closed cup
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C B'Hymer
Journal of chromatographic science, 45(6), 293-297 (2007-07-14)
An automated static headspace gas chromatographic method for the determination of residual solvents in the bulk drug substance alpha-phenyl-1-(2-phenylethyl)-piperine methanol, a serotonin 5-HT2 receptor antagonist, is evaluated. The method includes the use of 1-propanol as an internal standard. The gas
C B'Hymer
Journal of chromatographic science, 46(5), 369-374 (2008-05-22)
A static headspace gas chromatographic method is developed and evaluated for the quantitation of residual 2-propanol, methanol, and toluene in bulk (2alpha, 6alpha, 8alpha, 9alpha beta)-octahydro-3-oxo-2,6-methanon-2H-quinolizin-8-yl-1H-indole-3-caboxylate methanesufonate hydrate, a serotonin 5-HT3 receptor antagonist drug compound. This method is accurate and
P J Streete et al.
The Analyst, 117(7), 1111-1127 (1992-07-01)
Headspace gas chromatography with split flame-ionization-electron-capture detection is a simple method of screening for a wide range of volatile substances in biological fluids. A 60 m x 0.53 mm i.d. thick-film (5 microns) fused-silica capillary coated with SPB-1 (Supelchem) with
A Paraneeiswaran et al.
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Ilme Liblikas et al.
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The four possible isomers of tetradeca-4,8-dien-1-yl acetate and corresponding alcohols were synthesized stereoselectively by synthetic routes employing Wittig coupling reaction for the preparation of (Z,E)- and (Z,Z)-isomers, and alkylation of terminal alkynes for the preparation of (E,E)- and (E,Z)-isomers as
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