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Merck
CN

25420-U

SPB®-5 Capillary GC Column

L × I.D. 30 m × 0.53 mm, df 1.00 μm

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About This Item

UNSPSC Code:
41115710
NACRES:
SB.54
eCl@ss:
32119290
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material

fused silica

Quality Level

agency

meets requirements for USP G27 and G36

parameter

-60-300 °C temperature (isothermal), -60-320 °C temperature (programmed)

Beta value

133

df

1.00 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

30 m × 0.53 mm

matrix active group

SPB 5, Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

column type

capillary non-polar

General description

Capillary GC column is also known as open tubular column. The carrier gas flows through the central aperture and is unrestricted throughout the length of the column.
Application: This non-polar general purpose column provides primarily a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded
  • Poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D., <2 μm: -60 °C to 320 °C (isothermal or programmed)
  • ≤0.32 mm I.D., ≥2 μm: -60 °C to 300 °C (isothermal or programmed)
  • ≥0.53 mm I.D., <2 μm: -60 °C to 300 °C (isothermal) or 320 °C (programmed)
  • ≥0.53 mm I.D., ≥2 μm: -60 °C to 260 °C (isothermal) or 280 °C (programmed)

Application

SPB®-5 Capillary GC Column may be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany


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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
P M Scott et al.
Journal - Association of Official Analytical Chemists, 69(5), 889-893 (1986-09-01)
Nivalenol (NIV) is an important Fusarium mycotoxin shown to occur naturally in grains from several countries. Extraction and cleanup procedures previously described for trichothecene analysis have been modified to give good recoveries of NIV from cereal products. The extraction solvent
Determination of sterols by capillary column gas chromatography. Differentiation among different types of olive oil: virgin, refined, and solvent-extracted.
Jimenez O and Gonzalez ADV.
Journal of the American Oil Chemists' Society, 73 (12), 1685-1689 (1996)



Global Trade Item Number

SKUGTIN
25420-U04061825983806