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Merck
CN

G001688

US EPA Method 8270 (Appendix IX): GC Analysis of Semivolatiles on Equity-5 (30 m x 0.25 mm I.D., 0.50 μm)

suitable for GC

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technique(s)

gas chromatography (GC): suitable

test parameters

column: Equity-5, 30 m × 0.25 mm I.D., 0.5 μm (28092-U)
oven: 40 °C (2 min), 50 °C/min to 100 °C, 10 °C/min to 200 °C, 30 °C/min to 325 °C (7.5 min)
inj. temp.: 280 °C, splitless (0.61 min)
detector: MSD, Scan range 45-450 amu, 325°C
carrier gas: helium, pressure programmed, 20 psi (0.0 min), ramp to 80 psi (0.0 min), ramp to 16.5 psi (3 min), ramp to 25 psi (hold for remainder of run)
injection: 1 μL, splitless (0.61 min)
liner: 4 mm I.D., single taper
sample: 50 ng on-column of a 62 Supplemental Appendix IX list consisting of semivolatile standards, 6 internal standards, and 8 surrogates

application(s)

environmental

Legal Information

Analyte

Description
    Pentachloronitrobenzene
    3-Methylcholanthrene
    Methyl methanesulfonate
    1-Methylnaphthalene
    2,4,6-Tribromophenol
    7,12-Dimethylbenz[a]anthracene
    Diphenylamine
    Famphur
    Phenacetin
    3-Methylphenol, analytical standard
    2-Fluorobiphenyl
    Chlorobenzilate
    Pentachloroethane
    Thionazin
    o-Toluidine
    N-Nitrosodiethylamine
    Aniline
    1-Naphthylamine
    Acetophenone
    Hexachloropropene
    Parathion
    1,3-Dinitrobenzene
    Benzyl alcohol
    Naphthalene-d8
    Safrole
    1,4-Dinitrobenzene
    Nitrobenzene-d5
    Pentachlorobenzene
    α,α-Dimethylphenethylamine
    Methyl parathion, analytical standard
    Kepone
    1,3,5-Trinitrobenzene
    1,4-Dichlorobenzene-d4
    Ethyl methanesulfonate
    2-Fluorophenol
    5-Nitro-o-toluidine, analytical standard
    N-Nitrosopyrrolidine
    Perylene-d12
    Phenol-d6
    1,2-Dichlorobenzene-d4
    2,6-Dichlorophenol
    2,3,4,6-Tetrachlorophenol
    4-Nitroquinoline N-oxide
    Dibenz[a,h]acridine
    2-Picoline
    N-Nitrosomethylethylamine
    2-Naphthylamine
    1,4-Naphthoquinone
    4-Aminobiphenyl
    Pyridine
    Acenaphthene-d10
    Disulfoton
    Dinoseb
    Phorate
    1,2,4,5-Tetrachlorobenzene
    1,4-Dioxane
    2,3,5,6-Tetrachlorophenol
    Dimethoate
    See All (58)

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