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Merck
CN

G003579

US EPA Method 525.2: GC Analysis of Semivolatiles on SLB®-5ms

suitable for GC

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technique(s)

gas chromatography (GC): suitable

test parameters

column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 45 °C (1 min), 50 °C/min to 130 °C (1 min), 12 °C/min to 180 °C, 7 °C/min to 240 °C, 12 °C/min to 330 °C (2 min)
inj. temp.: 275 °C
MSD interface: 330 °C
scan range: m/z = 45-450
carrier gas: helium, 0.9 mL/min., constant flow
injection: 1 μL pulsed splitless (15 psi until 0.20 min) (1.0 min)
liner: 4 mm I.D., single taper
sample: 2 ppm, in ethyl acetate, of a 102 component semivolatile standard plus 3 surrogate and 3 internal standard compounds (at 5 ppm)

application(s)

environmental
food and beverages

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description

    Isophorone
    1,3-Dimethyl-2-nitrobenzene
    Dichlorvos
    Hexachlorocyclopentadiene
    EPTC, PESTANAL®, analytical standard
    Mevinphos
    Dimethyl phthalate
    Etridiazole
    2,6-Dinitrotoluene
    Acenaphthylene
    Acenaphthene-d10
    2-Chlorobiphenyl
    Tebuthiuron
    2,4-Dinitrotoluene
    Diethyl phthalate
    Fluorene
    Propachlor
    Cycloate
    Trifluralin
    α-BHC
    2,3-Dichlorobiphenyl
    Hexachlorobenzene
    Atraton
    Prometon
    Atrazine
    Propazine
    β-BHC
    Pentachlorophenol
    Terbufos
    Diazinon
    Disulfoton
    Chlorothalonil
    Phenanthrene
    Terbacil
    Anthracene
    δ-BHC
    2,4′,5-Trichlorobiphenyl
    Metribuzin
    Alachlor
    Simetryn
    Ametryn
    Prometryn
    Heptachlor
    Terbutryn
    Di-n-butyl phthalate, analytical standard, ampule of 5000 mg
    Bromacil
    2,2′,4,4′-Tetrachlorobiphenyl
    Metolachlor
    Cyanazine
    Aldrin
    Diphenamid
    MGK 264, PESTANAL®, analytical standard
    Heptachlor epoxide, PESTANAL®, analytical standard, isomer B
    2,2′,3′,4,6-Pentachlorobiphenyl
    α-Chlordane
    Butachlor
    Fenamiphos
    γ-Chlordane
    Pyrene
    1,1-Dichloro-2,2-bis(4-chlorophenyl)ethene
    2,2′,4,4′,5,6′-Hexachlorobiphenyl
    Dieldrin
    Endrin
    Chlorobenzilate
    4,4′-DDD, PESTANAL®, analytical standard
    Endrin aldehyde
    Norflurazon, PESTANAL®, analytical standard
    Endosulfan sulfate
    4,4′-DDT
    Hexazinone
    Bis(2-ethylhexyl) adipate
    Methoxychlor
    Triphenyl phosphate
    Endrin ketone
    2,2′,3,3′,4,4′,6-Heptachlorobiphenyl
    2,2′,3,3′,4,5′,6,6′-Octachlorobiphenyl
    Benz[a]anthracene
    Chrysene
    Bis(2-ethylhexyl) phthalate
    Fenarimol
    Benzo[b]fluoranthene
    Benzo[k]fluoranthene
    Benzo[a]pyrene
    Perylene-d12
    Indeno[1,2,3-cd]pyrene
    Dibenz[a,h]anthracene
    See All (86)

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