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Merck
CN

G006166

LC/MS Analysis of 2C Amines Drugs of Abuse on Ascentis® Express HILIC

application for HPLC

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technique(s)

HPLC: suitable

test parameters

column: Ascentis Express HILIC, 10 cm x 2.1 mm I.D., 2.7 μm particles (53939-U)
mobile phase: 5 mM ammonium formate in acetonitrile:water (90:10, v/v)
flow rate: 0.4 mL/min
column temp.: 35 °C
detector: TOF/MS
detector: 2.0 μL
sample: 300 ng/mL in acetonitrile

suitability

application for HPLC

application(s)

clinical
forensics and toxicology

Legal Information

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    (R)-(-)-Bromo-DragonFLY hydrochloride solution, 1 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®
    (±)-2,5-Dimethoxy-4-Iodoamphetamine hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®
    (±)-2,5-Dimethoxy-4-bromoamphetamine hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®
    2C-B-FLY hydrochloride solution, 1 mg/mL in acetonitrile: water (9:1), ampule of 1 mL, certified reference material, Cerilliant®

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