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G006168

US EPA Method TO-17: GC Analysis of Volatiles on Equity™-1 after Collection/Desorption using Carbotrap 300 Tube

suitable for GC

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technique(s)

gas chromatography (GC): suitable

test parameters

thermal desorption tube: Carbotrap® 300 glass TD tube, fritted, O.D. × L 1/4 in. × 3 1/2 in., unconditioned, pkg of 10 ea (30141-U)
sample/matrix: TO15/17 Calibration Mix, 1 PPM in N2 (41973-U)
dry purge: 1 min
bake: 350 °C
transfer line/valve temp.: 175 °C
column: FS CAP Equity-1 30 m x 0.25 mm I.D. x 1.0 μm (28049-U)
oven: 40 °C/8 min to 100 °C @ 5 °C/min to 220 °C @ 15 °C/min, hold for 10 min
detector: MSD
MSD interface: 175 °C
scan range: 35-265
carrier gas: Helium

application(s)

environmental
industrial hygiene

Analysis Note

This application shows the chromatography achieved using an Equity-1 column.

Legal Information

Carbotrap is a registered trademark of Merck KGaA, Darmstadt, Germany
Equity is a trademark of Sigma-Aldrich Co. LLC

Analyte

Description
    1,2-Dichlorotetrafluoroethane
    1,3-Butadiene
    Ethanol
    Chloroethane
    Acetone
    Trichlorofluoromethane
    2-Propanol
    1,1-Dichloroethylene
    Dichloromethane
    1,1,2-Trichloro-1,2,2-trifluoroethane
    Carbon disulfide
    1,1-Dichloroethane
    tert-Butyl methyl ether
    2-Butanone
    trans-1,2-Dichloroethylene
    Ethyl acetate
    Chloroform
    Tetrahydrofuran
    1,2-Dichloroethane
    1,1,1-Trichloroethane
    Benzene
    Carbon tetrachloride
    Cyclohexane
    1,2-Dichloropropane
    Bromodichloromethane
    Trichloroethylene
    cis-1,3-Dichloropropene
    4-Methyl-2-pentanone
    trans-1,3-Dichloropropene
    Toluene
    Dibromochloromethane
    1,2-Dibromoethane
    Tetrachloroethylene
    Chlorobenzene
    Bromoform
    m-Xylene
    p-Xylene
    Styrene
    o-Xylene
    1,1,2,2-Tetrachloroethane
    Mesitylene
    1,2,4-Trimethylbenzene
    1,3-Dichlorobenzene
    Benzyl chloride
    1,4-Dichlorobenzene
    1,2-Dichlorobenzene
    1,2,4-Trichlorobenzene
    Hexachloro-1,3-butadiene
    See All (48)

analytical column

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