SnCl2/TiCl3-mediated deoximation of oximes in an aqueous solvent.

SnCl2/TiCl3-mediated deoximation of oximes in an aqueous solvent.

Molecules (Basel, Switzerland) (2012-03-03)

Mei-Huey Lin, Han-Jun Liu, Cheng-Yu Chang, Wei-Cheng Lin, Tsung-Hsun Chuang

ABSTRACT

A simple procedure for SnCl(2)/TiCl(3)-mediated deoximation of ketoximes in an aqueous solvent is reported. Under the conditions developed in this effort, various ketones and aldehydes are produced in good to excellent yields.

MATERIALS

Product Number

Brand

Product Description

42163

Supelco

Acetophenone, analytical standard

A10701

Sigma-Aldrich

Acetophenone, ReagentPlus^®, 99%

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