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Calibration, qualification, and validation

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facet applications:Calibration, qualification, and validation
facet content type:Protocol
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Sildenafil Citrate Method (HPLC) following USP Monograph on Ascentis® Express C18 with UV detection
Sildenafil, sold under the brand name Viagra, among others, is a medication used to treat erectile dysfunction and pulmonary arterial hypertension.
Analysis of Fipronil and Fipronil Sulfone in Eggs, Chicken Meat and Mayonnaise
A short abstract on a method using QuEChERS and GC/MS/MS for determination of fipronil & fipronil sulfone.
ENVI-Carb Plus for the Extraction of Propylene Glycol and Ethylene Glycol from Water
ENVI-Carb Plus for the Extraction of Propylene Glycol and Ethylene Glycol from Water
GC Analyses of FAMEs by Boiling Point Elution
GC Analyses of FAMEs by Boiling Point Elution
HPLC Analysis of Insulin Variants and Analogs
Chromatographic technique identifies insulin variants efficiently, aiding in pharmacokinetics.
Capillary GC Columns for GC x GC
GCxGC excels in compound resolution, making it indispensable in analytical chemistry for complex samples.
Determination of Free and Total Glycerin in B100
Glycerin determination methods require multi-component calibration solutions for accurate analysis.
HPTLC for Passiflora incarnata
HPTLC fingerprinting enables rapid identification of passion flower with related reference materials.
PAHs Determination in Paprika Powder using SPE
Paprika spice's PAH contamination risk due to environmental exposure highlights food safety concerns.
Fast GC for Trans FAME Analysis
Fast GC analysis utilizes short capillary columns, H2 carrier gas, and rapid temperature programming rates.
Analysis of Active Cannabis Compounds
HPLC-UV analysis of active compounds in marijuana-infused edibles for potency testing; complex matrix requires precise methods.
UHPLC/MS for Drug Detection in Urine
Optimize β-glucuronidase hydrolysis for glucuronide metabolite analysis considering factors like time, temperature, pH, and enzyme concentration.
Bisphenol A Analysis in Food by SPME
Overcoated SPME fiber enables low-level BPA analysis in food via SPME-GC-MS/MS, meeting tighter migration limit regulations.
Fast and Reliable Environmental Analysis of Aldehyde and Ketone Air Pollutants
Aldehydes and ketones are ubiquitous air pollutants. Along with esters and ethers, they are major components of indoor air pollution and are therefore important for industrial hygiene applications.
Sildenafil Citrate USP Method Using HPTLC Plates for the Limit of Imidazole Test
In the present study we demonstrate compliance of silica gel 60 F254 HPTLC plates with USP requirements, and how HPTLC plates are suitable for the Sildenafil citrate-Limit of Imidazole test.
EN 14105: GC Analysis of Glycerin Impurity in Biodiesel on MET-Biodiesel
EN 14105: GC Analysis of Glycerin Impurity in Biodiesel on MET-Biodiesel
GC Analysis of Bacterial Acid Methyl Esters (BAMEs) on Equity®-1
Protocol for GC Analysis of Bacterial Acid Methyl Esters (BAMEs) on Equity®-1
New GC-MS Method for Mycotoxin Analysis
An article regarding A New GC-MS Method for Mycotoxin Analysis Using 13C-marked Mycotoxin Derivatives from Sigma-Aldrich.com
Extraction and Analysis of Lasix (Furosemide) in Horse Serum
Studies have suggested that there is a correlation between furosemide and improved racing performance, prompting the horse racing industry to monitor the use of this drug
Developing a Quantitative SPME Method
Developing a Quantitative SPME Method
Quantitative NMR for Content Assignment of Reference Standards for Quality Control of Herbal Medicinal Products
qNMR has proven to be appropriate as a primary analytical method for the certification of natural products as reference standards for QC of herbal medicinals.
Derivatization of Fatty acids to FAMEs
Explore how GC can be used to analyze fatty acids either as free fatty acids or as fatty acid methyl esters.
GC Analysis of Grob Test Mix SLB IL76i
GC Analysis of Grob Test Mix on SLB®-IL76i
GC Analyses of Free Fatty Acids
GC Analyses of Free Fatty Acids
GC Analysis of FAMEs in Five Edible Oils (Canola, Lard, Palm, Soybean, and Sunflower Seed) on SLB®-IL111
GC Analysis of FAMEs in Five Edible Oils (Canola, Lard, Palm, Soybean, and Sunflower Seed) on SLB®-IL111
Analysis of Isocyanates Using the ASSET™ EZ4-NCO Dry Sampler
The unique sampler design ensures that both the vapor phase and particulate isocyanates are captured and derivatized during sampling.
FAME Standard for Optimizing GC System Performance
AOCS and AOAC methods for determining the trans fatty acid composition of foods by gas chromatography require the use of a highly polar cyanosilicone capillary column to provide the best peak resolution attainable of the numerous geometric (cis & trans)
GC Analysis of a 37-Component FAME Mix on SP™-2560
A protocol for GC Analysis of a 37-Component FAME Mix on SP™-2560.
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