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  • Pesticide residues in orange fruit from citrus orchards in Nuevo Leon State, Mexico.

Pesticide residues in orange fruit from citrus orchards in Nuevo Leon State, Mexico.

Food additives & contaminants. Part B, Surveillance (2017-04-05)
Angela Suárez-Jacobo, Victor Manuel Alcantar-Rosales, Diana Alonso-Segura, Maria Heras-Ramírez, Dalau Elizarragaz-De La Rosa, Ofelia Lugo-Melchor, Octavio Gaspar-Ramirez
ABSTRACT

Some international organisations established maximum residue limits (MRLs) in food to protect human health. Mexico lacks regulations in this matter, affecting national and international trade from agroindustry. The aim of this study was to diagnose pesticide residues in oranges from Nuevo Leon, México, in citrus orchards. In May 2014, 100 orange fruit samples were taken randomly from orchards and subjected to analysis for 93 pesticides at residual level by GC/QQQ-MS and LCQ-TOF-MS. Results showed the presence of 15 pesticide residues in the samples. The comparison of the residual levels of pesticides found in orange samples among the MRLs allowed by USA, EU and Japanese regulations demonstrated that all samples were below MRLs issued by USA and Japan. Some orange samples were above MRLs issued by the EU. This provides a basis to establish strategies in order to satisfy International Standards to protect human health and encourage Food Safety in Mexico.

MATERIALS
Product Number
Brand
Product Description

Supelco
Chlorfenapyr, PESTANAL®, analytical standard
Supelco
Diflubenzuron, PESTANAL®, analytical standard
Supelco
Fenamiphos, PESTANAL®, analytical standard
Supelco
Quinalphos, PESTANAL®, analytical standard
Supelco
Phosmet, PESTANAL®, analytical standard
Supelco
Pyridaben, PESTANAL®, analytical standard
Supelco
Fenoxycarb, PESTANAL®, analytical standard
Supelco
Acephate, PESTANAL®, analytical standard
Supelco
Etofenprox, PESTANAL®, analytical standard
Supelco
Tebufenozide, PESTANAL®, analytical standard
Supelco
Fludioxonil, PESTANAL®, analytical standard
Supelco
Coumaphos, PESTANAL®, analytical standard
Supelco
Phorate, PESTANAL®, analytical standard
Supelco
Spirodiclofen, PESTANAL®, analytical standard
Supelco
Terbufos, PESTANAL®, analytical standard
Supelco
Pyriproxyfen, PESTANAL®, analytical standard
Supelco
Tebuthiuron, PESTANAL®, analytical standard
Supelco
Bromopropylate, PESTANAL®, analytical standard
Supelco
Methiocarb, PESTANAL®, analytical standard
Supelco
N-(6-Chloro-3-pyridylmethyl)-N-cyano-N-methylacetamidine, PESTANAL®, analytical standard
Supelco
Flufenoxuron, PESTANAL®, analytical standard
Supelco
Fenpyroximate, PESTANAL®, analytical standard
Supelco
Tebuconazole, PESTANAL®, analytical standard
Supelco
Pyrimethanil, PESTANAL®, analytical standard