2 mL water + sodium chloride at 25% (pH 11) containing each analyte at 5 ppm, in a 4 mL vial
85 μm Polyacrylate, 24 ga (57304)
eated headspace, 60 °C for 5 min
250 °C for 3 min
Equity-1, 10 m x 0.20 mm I.D., 1.2 μm (28043-U)
40 °C (0.75 min), 20 °C/min to 200 °C (10 min)
250 °C
FID
helium, 35 cm/sec @ 40 °
5:1 split
0.75 mm I.D. SPME type
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