2 mL water + sodium chloride at 25% (pH 11) containing each analyte at 5 ppm, in a 4 mL vial
85 μm Polyacrylate (57304)
heated headspace, 60 °C for 5 min
250 °C for 3 min
VOCOL, 10 m x 0.20 mm I.D., 1.2 μm (24129-U)
40 °C (0.75 min), 20 °C/min to 200 °C (10 min)
250 °C
FID
helium, 35 cm/sec @ 40 °C
5:1 split
0.75 mm I.D. SPME type
VOCOL is a registered trademark of Merck KGaA, Darmstadt, Germany