0.7 mL water spiked with 2-600 μg/liter each analyte, 0.25 g NaCl added
30 μm PDMS (57309)
headspace, 12 sec (no stirring), ambient temp.
2-3 min, 250 °C (0.75-1.0 mm I.D. inj. port liner)
Equity-1, 10 m × 0.20 mm I.D., 1.2 μm (available on request)
70 °C (0.2 min) to 180 °C at 50 °C/min
FID, 250 °C
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