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US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SLB®-5ms (15 m x 0.10 mm I.D., 0.10 μm), Fast GC Analysis

US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SLB®-5ms (15 m x 0.10 mm I.D., 0.10 μm), Fast GC Analysis suitable for GC

Materials

analytical column

Product No.
Description
Pricing

24103-U

SPB®-608 Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

25312

SPB®-608 Capillary GC Column

L × I.D. 30 m × 0.53 mm, df 0.50

28372-U

Equity™-1701 Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

28378-U

Equity™-1701 Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 1.00 μm

28391-U

Equity™-1701 Capillary GC Column

L × I.D. 30 m × 0.53 mm, df 0.50 μm

28471-U

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

28476-U

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 1.00 μm

28466-U

SLB®-5ms Capillary GC Column

L × I.D. 15 m × 0.10 mm, df 0.10 μm

accessory

Product No.
Description
Pricing

Z250228

Wheaton wide-mouth bottle

capacity 32 oz (1000 mL), white polypropylene cap, PTFE flat liner, amber

guard column

Product No.
Description
Pricing

25740-U

Non-Polar Fused Silica Tubing

L × I.D. 5.0 m × 0.10 mm

25742

Non-Polar Fused Silica Tubing

L × I.D. 5.0 m × 0.25 mm

25744

Non-Polar Fused Silica Tubing

L × I.D. 5.0 m × 0.53 mm

recommended

Product No.
Description
Pricing

23817

Polyimide Sealing Resin

pkg of 5 g

required but not provided

Product No.
Description
Pricing

20480

"Y" GlasSeal™ Connector, Borosilicate Glass

pkg of 1 ea

23631

"Y" GlasSeal™ Connector, Fused Silica

pkg of 1 ea

23632

"Y" GlasSeal™ Connector, Fused Silica

pkg of 3 ea

standard

Product No.
Description
Pricing

48065-U

Chlordane (mixture of isomers)

certified reference material, 1000 μg/mL in isooctane

48458

Pesticides Matrix Spike Mix

in methanol (varied), PESTANAL®, analytical standard

48103

Toxaphene solution

certified reference material, 1000 μg/mL in isooctane

CRM48460

Pesticide Surrogate Spike Mix

certified reference material, TraceCERT®, 200 μg/mL each component in acetone, ampule of 1 mL

CRM47426

EPA CLP Organochlorine Pesticide MIx

certified reference material, 2000 μg/mL each component in hexane: toluene (1:1), ampule of 1 mL

CONDITIONS

column

SLB-5ms, 15 m × 0.10 mm I.D., 0.10 μm (28466-U)

oven

100 °C, 25 °C/min to 325 °C

inj. temp.

225 °C

detector

ECD, 300 °C

carrier gas

hydrogen, 40 cm/sec constant

injection

2 μL, splitless (0.75 min)

liner

4 mm I.D., single taper

sample

50 ppb of a 22 component chlorinated pesticide standard in n-hexane

Description

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

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