US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB^®-5ms (20 m x 0.18 mm I.D., 0.36 μm), Fast GC Analysis

column

SLB-5ms, 20 m x 0.18 mm I.D., 0.36 μm (28576-U)

oven

100 °C (2 min), 15 °C/min to 325 °C (3 min)

inj. temp.

250 °C

detector

micro-ECD, 325 °C

carrier gas

helium, 0.5 mL/min, constant flow

injection

1.0 μL, splitless (0.75 min)

liner

4 mm I.D., single taper

sample

Aroclor standard mix 1 (46846-U) diluted to 500 ppb / 50 ppb (Aroclors / surrogates) in n-hexane