each analyte at 50 ppb in 5 mL water
VOCARB 3000 “K”
40 mL/min at 25 °C for 11 min
2 min
205 °C
150 mL/min at 210 °C for 2 min
260 °C for 10 min
110 °C
VOCOL, 20 m × 0.18 mm I.D., 1.0 μm (28463-U)
40 °C (0.8 min), 19 °C/min to 125 °C, 32 °C/min to 220 °C (1 min)
150 °C
200 °C
m/z = 35-400
helium, 1.4 mL/min
100:1 split
0.75 mm I.D. SPME
VOCOL is a registered trademark of Merck KGaA, Darmstadt, Germany