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HPLC Analysis of Aminoglutethimide Enantiomers on Astec® Cellulose DMP

HPLC Analysis of Aminoglutethimide Enantiomers on Astec® Cellulose DMP application for HPLC

Materials

related product

Product No.
Description
Pricing

DL-Aminoglutethimide

Astec® Cellulose DMP Chiral HPLC Column

5 μm particle size, L × I.D. 25 cm × 4.6 mm

used together

Product No.
Description
Pricing

2-Propanol

99.5%, HPLC grade

Diethylamine

≥99.5%

CONDITIONS

column

Astec Cellulose DMP; 25 cm x 4.6 mm I.D., 5 μm particles (51099AST)

mobile phase

[A] heptane; [B] isopropanol; [C] diethylamine; (70:30:0.1, A:B:C)

flow rate

1 mL/min

column temp.

30 °C

injection

15 μL

sample

aminoglutethimide, 1 g/L in 50:50, heptane:isopropanol

Description

Analysis Note

Aminoglutethimide enantiomers are resolved by normal phase chromatography.

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany