LC/MS Analysis of Antifungals on Ascentis® Express Phenyl-Hexyl

Materials
related product
Product No.
Description
Pricing
Fluconazole solution
2.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®Itraconazole solution
2.0 mg/mL (Methanol with 1% 1M HCl), ampule of 1 mL, certified reference material, Cerilliant®Posaconazole solution
2.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®Voriconazole solution
2.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®Ketoconazole solution
2.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®used together
Product No.
Description
Pricing
CONDITIONS
column
Ascentis Express Phenyl-Hexyl, 10 cm x 2.1 mm I.D., 2.7 μm particles (53336-U)
gradient
[A] 10 mM ammonium acetate; [B] acetonitrile
gradient
2% B for 1 min; to 100% B in 10 min; held at 100% B for 1 min
flow rate
0.3 mL/min
pressure
2930 psi (202 bar)
column temp.
35 °C
detector
MS, ESI+, XIC
injection
0.5 μL
sample
Antifungals, 1-10 μg/mL in 99:1, water:methanol
Description
Legal Information
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany