UHPLC Analysis of Flakka and Related Compounds on Titan Silica in HILIC Mode
Materials
related product
Product No.
Description
Pricing
3,4-Methylenedioxypyrovalerone HCl (MDPV) solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®MDPBP hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®Naphyrone hydrochloride
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®α-Pyrrolidinovalerophenone hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®α-Pyrrolidinopropiophenone hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®CONDITIONS
column
Titan Silica, 10 cm x 2.1 mm I.D., 2 μm (581532-U)
mobile phase
10 mM ammonium formate in acetonitrile:water (95:5)
flow rate
0.4 mL/min
column temp.
35 °C
detector
UV, 265 nm
injection
1 μL
sample
50 μg/mL in methanol:acetonitrile (10:90)
Description
Analysis Note
The rapid separation of the street drug Flakka (α-PVP) and related compounds is shown here on a Titan Silica column in HILIC mode. Highest grade UHPLC solvents were used to supply low background interference and low particulate contamination for robust, trouble-free operation. Cerilliant CRMs provided reliable identification and quantification.
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