Skip to Content
Merck
CN

LC/MS Analysis of Tobacco Nitrosamines on Ascentis® Express OH5

LC/MS Analysis of Tobacco Nitrosamines on Ascentis® Express OH5 application for LC-MS

Materials

related product

Product No.
Description
Pricing

(±)-N′-Nitrosonornicotine (NNN) solution

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

4-(Methylnitrosamino)-1-(3-pyridyl)-1-butanone (NNK) solution

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

(S)-N-Nitrosoanabasine (NAB) solution

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

(S)-N-Nitrosoanatabine solution

1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

Ascentis® Express OH5, 2 μm UHPLC Column

2 μm particle size, L × I.D. 10 cm × 3 mm

CONDITIONS

column

Ascentis Express OH5 10 cm x 3.0 mm, 2.0 μm particles (50967-U)

mobile phase

0.1% Formic acid in 95:5, acetonitrile:water

flow rate

0.4 mL/min

pressure

3145 psi (217 bar)

column temp.

25 °C

detector

MS ESI+; SIR

injection

3 μL

sample

500 ng/mL in acetonitrile

Description

Legal Information

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany