UHPLC/MS Analysis of Spice Cannabinoid Metabolites in Urine on Titan C18
Materials
related product
Product No.
Description
Pricing
JWH-018 5-Pentanoic acid metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®JWH-018 4-Hydroxypentyl metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®JWH-073 4-Butanoic acid metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®JWH-073 N-(3-hydroxybutyl) metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®JWH-250 5-Hydroxypentyl metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®JWH-250 4-Hydroxypentyl metabolite
ampule of 1 mL, certified reference material, 100 μg/mL in methanol, Cerilliant®JWH-122 4-Hydroxypentyl metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®JWH-122 5-Hydroxypentyl metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®JWH-210 5-Hydroxypentyl metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®JWH-210 4-Hydroxypentyl metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®JWH-073 4-Hydroxybutyl metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®JWH-018 5-Hydroxypentyl metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®AM2201 4-Hydroxypentyl metabolite solution
100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®used together
Product No.
Description
Pricing
CONDITIONS
sample preparation
SPE (Solid Phase Extraction)
SPE well plate
SupelSelect HLB 96-Well Plate, 60mg/well (575662-U)
condition
1 mL methanol, then 1 mL water
sample addition
100 ng/mL in matrix
drying
none
washing
1 mL 20% methanol in water
elution
2 mL methanol
eluate post-treatment
none
column
Titan C18 10 cm x 2.1 mm, 1.9 μm particles (577124-U)
mobile phase
[A] 0.1% formic acid in 95:5, water:acetonitrile; [B] 0.1% formic acid in 5:95, water:acetonitrile;
gradient
25% B held for 1 min; to 45% B in 0.5 min; 45% B held for 4.5 min; to 80% B in 0.5 min; 80% B held for 4 min
flow rate
0.5 mL/min
pressure
8756 psi (604 bar)
temp.
35 °C
detector
MS-ESI+,100 - 1000 m/z scan, XIC
injection
2 μL
sample
100 ng/mL in methanol
Description
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