产品名称
2-氨基苯乙醇, 97%
Quality Level
InChI key
ILDXSRFKXABMHH-UHFFFAOYSA-N
InChI
1S/C8H11NO/c9-8-4-2-1-3-7(8)5-6-10/h1-4,10H,5-6,9H2
SMILES string
Nc1ccccc1CCO
assay
97%
refractive index
n20/D 1.588 (lit.)
bp
147-148 °C/3.5 mmHg (lit.)
density
1.045 g/mL at 25 °C (lit.)
functional group
hydroxyl
Application
2-氨基苯乙醇用于以下物质的合成：
- 吲哚衍生物
- N-（氰基硫代甲酰基）二氢吲哚
- 二氢-3,1-苯并恶嗪
General description
2-氨基苯乙醇在PPh3、CCl4和Net33的存在下与羧酸进行一锅环化反应，生成 N-酰基二氢吲哚。
Other Notes
这种材料可能会随着时间变黑，但对化学纯度的影响很小。
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
存储类别
11 - Combustible Solids
wgk
WGK 3
flash_point_f
235.4 °F - closed cup
flash_point_c
113 °C - closed cup
ppe
dust mask type N95 (US), Eyeshields, Gloves
N-(Cyanothioformyl) indoline; a new indoline ring forming reaction.
Besson T, et al.
Journal of the Chemical Society. Perkin Transactions 1, 24, 4057-4060 (1998)
Zengxue Wang et al.
The Journal of organic chemistry, 72(24), 9364-9367 (2007-11-02)
A unique one-pot cyclization of 2-aminophenethyl alcohols with carboxylic acids in the presence of PPh3, CCl4, and NEt3 furnished the formation of N-acyl indolines in good to excellent yields. This new approach provides an efficient, scalable, low-cost, and direct access
Ruthenium-catalyzed dehydrogenative N-heterocyclization. Indoles from 2-aminophenethyl alcohols and 2-nitrophenethyl alcohols.
Tsuji Y, et al.
The Journal of Organic Chemistry, 55(2), 580-584 (1990)
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