416436
二苄基 N,N-二异丙基亚磷酰胺
technical grade, 90%
别名:
N,N-二异丙基二苄基磷酰胺, [双(苄氧基)膦基]双(丙烷-2-基)胺, 二苄基N,N-二异丙基磷酰胺, 二苄基二异丙基磷酰胺, 双(苄氧基)(二异丙基氨基)膦
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关于此项目
线性分子式:
[(CH3)2CH]2NP(OCH2C6H5)2
化学文摘社编号:
分子量:
345.42
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
MDL number:
Beilstein/REAXYS Number:
3616864
Assay:
90%
Form:
liquid
InChI
1S/C20H28NO2P/c1-17(2)21(18(3)4)24(22-15-19-11-7-5-8-12-19)23-16-20-13-9-6-10-14-20/h5-14,17-18H,15-16H2,1-4H3
SMILES string
CC(C)N(C(C)C)P(OCc1ccccc1)OCc2ccccc2
InChI key
ANPWLBTUUNFQIO-UHFFFAOYSA-N
grade
technical grade
assay
90%
form
liquid
refractive index
n20/D 1.535 (lit.)
bp
130 °C/0.55 mmHg (lit.)
solubility
THF: soluble(lit.), acetonitrile: soluble(lit.), cold water: insoluble(lit.), dichloromethane: soluble(lit.)
density
1.028 g/mL at 25 °C (lit.)
functional group
amine, phenyl
storage temp.
2-8°C
Quality Level
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Application
N,N-二异丙基亚磷酰胺基二苄基酯可用于制备磷酸肽。它可用于合成GDP（鸟苷二磷酸）类似物SML-8-73-1。
存储类别
10 - Combustible liquids
wgk
WGK 3
flash_point_f
156.2 °F - closed cup
flash_point_c
69 °C - closed cup
ppe
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
D L Clemm et al.
Molecular endocrinology (Baltimore, Md.), 14(1), 52-65 (2000-01-11)
Human progesterone receptor (PR) is phosphorylated on multiple serine residues (at least seven sites) in a manner that involves distinct groups of sites coordinately regulated by hormone and different kinases. Progress on defining a functional role for PR phosphorylation has
D M Andrews et al.
International journal of peptide and protein research, 38(5), 469-475 (1991-11-01)
A completely general method for the O-phosphorylation of peptides of any given composition using solid-phase methodology is described. Peptides were assembled using Fmoc amino acid active esters, with base used for Fmoc deprotection. Unprotected amino acid side chain hydroxyl groups
Sang Min Lim et al.
Angewandte Chemie (International ed. in English), 53(1), 199-204 (2013-11-22)
We report the synthesis of a GDP analogue, SML-8-73-1, and a prodrug derivative, SML-10-70-1, which are selective, direct-acting covalent inhibitors of the K-Ras G12C mutant relative to wild-type Ras. Biochemical and biophysical measurements suggest that modification of K-Ras with SML-8-73-1
Jie Xue et al.
Organic letters, 6(9), 1365-1368 (2004-04-23)
[reaction: see text] A new one-step reaction has been developed for converting 4-azido-4-deoxy-d-galactoside into 4-deoxy-d-erythro-hexos-3-ulose by phosphoramidites and tetrazole. It is proposed that the new reaction proceeds via an intramolecular Staudinger reaction of the phosphite intermediate and a tetrazole-catalyzed elimination
Synthesis, 9, 1481-1485 (2004)
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