等级
derivatization grade ((GC derivatization))
derivatization grade
描述
Silylation reagent
表单
liquid
反应适用性
reagent type: derivatization reagent
reaction type: Acylations
reagent type: derivatization reagent
reaction type: Silylations
包装
pkg of 100 mL
技术
GC/MS: suitable
一般描述
Chlorotrimethylsilane is widely used in characterising organolithium compounds. It is also used in establishing the degree of polymetallation by organolithium compounds.
应用
It was used to reconstitute the phytic acid residue during derivatization procedure, before injecting the residue into GC for determination of phytic acid content in biological samples. It was also used in toluene for silanizing all the glassware used for detecting, identifying and quantifying polychlorinated biphenyls (PCB) using solid-phase microextraction combined with gas chromatography with electron capture detection.
其他说明
Reagent for trimethylsilyl chlorohydrin, trimethylsilyl and trimethylsilyl ether.
警示用语：
Danger
危险分类
Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Acute Tox. 4 Dermal - Eye Dam. 1 - Flam. Liq. 2 - Skin Corr. 1A
补充剂危害
储存分类代码
3 - Flammable liquids
WGK
WGK 1
闪点(°F)
-18.4 °F - closed cup
闪点(°C)
-28 °C - closed cup
个人防护装备
Faceshields, Gloves, Goggles
法规信息
新产品
此项目有
D.J.Harvey et al.
Analytical Letters, 3, 489-489 (1970)
J G March et al.
Journal of chromatography. B, Biomedical sciences and applications, 757(2), 247-255 (2001-06-22)
A GC-MS method is reported for the determination of phytic acid based on purification by anion-exchange chromatography, enzymatic hydrolysis of phytic acid to myo-inositol and derivation to trimethylsilyl derivative, with scyllo-inositol as an internal standard. Analytical features of the method
M.G.Horning et al.
Journal of Gas Chromatography, 5, 297-297 (1967)
B. J. Wakefield
The Chemistry of Organolithium Compounds, 260-260 (2013)
Jszafranek et al.
Journal of Chromatography A, 88, 149-149 (1974)
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