grade
derivatization grade ((GC derivatization)), derivatization grade
description
Silylation reagent
form
liquid
reaction suitability
reagent type: derivatization reagent
reaction type: Acylations, reagent type: derivatization reagent
reaction type: Silylations
packaging
pkg of 100 mL
technique(s)
GC/MS: suitable
General description
Chlorotrimethylsilane is widely used in characterising organolithium compounds. It is also used in establishing the degree of polymetallation by organolithium compounds.
Application
It was used to reconstitute the phytic acid residue during derivatization procedure, before injecting the residue into GC for determination of phytic acid content in biological samples. It was also used in toluene for silanizing all the glassware used for detecting, identifying and quantifying polychlorinated biphenyls (PCB) using solid-phase microextraction combined with gas chromatography with electron capture detection.
Other Notes
Reagent for trimethylsilyl chlorohydrin, trimethylsilyl and trimethylsilyl ether.
signalword
Danger
Hazard Classifications
Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Acute Tox. 4 Dermal - Eye Dam. 1 - Flam. Liq. 2 - Skin Corr. 1A
supp_hazards
存储类别
3 - Flammable liquids
wgk
WGK 1
flash_point_f
-18.4 °F - closed cup
flash_point_c
-28 °C - closed cup
ppe
Faceshields, Gloves, Goggles
法规信息
新产品
此项目有
D.J.Harvey et al.
Journal of the Chemical Society. Perkin Transactions 1, 1, 1074-1074 (1972)
O. Ceder and B. Hansson
Acta Chemica Scandinavica, B30, 574-574 (1976)
J F Kennedy et al.
Carbohydrate research, 57, 205-214 (1977-08-01)
The structures of the isomeric products obtained on trimethylsilylation of naturally occurring hexuronic acids and their sodium salts and lactones have been established by the application of n.m.r. (for anomeric configuration) and mass spectrometry (for ring size). The equilibria of
M.B.Perry et al.
Journal of Chromatography A, 44, 614-614 (1969)
B. J. Wakefield
The Chemistry of Organolithium Compounds, 260-260 (2013)
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