grade
derivatization grade ((GC derivatization)), derivatization grade
description
Silylation reagent
form
liquid
reaction suitability
reagent type: derivatization reagent
reaction type: Acylations, reagent type: derivatization reagent
reaction type: Silylations
packaging
pkg of 100 mL
technique(s)
GC/MS: suitable
General description
Chlorotrimethylsilane is widely used in characterising organolithium compounds. It is also used in establishing the degree of polymetallation by organolithium compounds.
Application
It was used to reconstitute the phytic acid residue during derivatization procedure, before injecting the residue into GC for determination of phytic acid content in biological samples. It was also used in toluene for silanizing all the glassware used for detecting, identifying and quantifying polychlorinated biphenyls (PCB) using solid-phase microextraction combined with gas chromatography with electron capture detection.
Other Notes
Reagent for trimethylsilyl chlorohydrin, trimethylsilyl and trimethylsilyl ether.
signalword
Danger
Hazard Classifications
Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Acute Tox. 4 Dermal - Eye Dam. 1 - Flam. Liq. 2 - Skin Corr. 1A
supp_hazards
存储类别
3 - Flammable liquids
wgk
WGK 1
flash_point_f
-18.4 °F - closed cup
flash_point_c
-28 °C - closed cup
ppe
Faceshields, Gloves, Goggles
法规信息
新产品
此项目有
Cláudia H Kowalski et al.
Talanta, 116, 315-321 (2013-10-24)
Due to the tendency of polychlorinated biphenyls (PCB) to accumulate in matrixes with high lipid content, the contamination of the breast milk with these compounds is a serious issue, mainly to the newborn. In this study, milk samples were collected
B. J. Wakefield
The Chemistry of Organolithium Compounds, 260-260 (2013)
D.R. Knapp
Handbook of Analytical Derivatization Reactions, 472-472 (1979)
Jszafranek et al.
Journal of Chromatography A, 88, 149-149 (1974)
M.B.Perry et al.
Journal of Chromatography A, 44, 614-614 (1969)
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