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Merck
CN

33014

三甲基氯硅烷

pkg of 100 mL

别名:

TMCS,衍生化级, TMCS, Trimethylchlorosilane, 三甲基硅基氯

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EC Number:
200-900-5
UNSPSC Code:
41116105
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grade

derivatization grade ((GC derivatization)), derivatization grade

description

Silylation reagent

form

liquid

reaction suitability

reagent type: derivatization reagent
reaction type: Acylations, reagent type: derivatization reagent
reaction type: Silylations

packaging

pkg of 100 mL

technique(s)

GC/MS: suitable

General description

Chlorotrimethylsilane is widely used in characterising organolithium compounds. It is also used in establishing the degree of polymetallation by organolithium compounds.

Application

It was used to reconstitute the phytic acid residue during derivatization procedure, before injecting the residue into GC for determination of phytic acid content in biological samples. It was also used in toluene for silanizing all the glassware used for detecting, identifying and quantifying polychlorinated biphenyls (PCB) using solid-phase microextraction combined with gas chromatography with electron capture detection.

Other Notes

Reagent for trimethylsilyl chlorohydrin, trimethylsilyl and trimethylsilyl ether.

signalword

Danger

Hazard Classifications

Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Acute Tox. 4 Dermal - Eye Dam. 1 - Flam. Liq. 2 - Skin Corr. 1A

supp_hazards

存储类别

3 - Flammable liquids

wgk

WGK 1

flash_point_f

-18.4 °F - closed cup

flash_point_c

-28 °C - closed cup

ppe

Faceshields, Gloves, Goggles

法规信息

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历史批次信息供参考:

分析证书(COA)

Lot/Batch Number

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Cláudia H Kowalski et al.
Talanta, 116, 315-321 (2013-10-24)
Due to the tendency of polychlorinated biphenyls (PCB) to accumulate in matrixes with high lipid content, the contamination of the breast milk with these compounds is a serious issue, mainly to the newborn. In this study, milk samples were collected
B. J. Wakefield
The Chemistry of Organolithium Compounds, 260-260 (2013)
D.R. Knapp
Handbook of Analytical Derivatization Reactions, 472-472 (1979)
Jszafranek et al.
Journal of Chromatography A, 88, 149-149 (1974)
M.B.Perry et al.
Journal of Chromatography A, 44, 614-614 (1969)

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