技术
gas chromatography (GC): suitable
试验参数
column: Equity-5, 30 m × 0.25 mm I.D., 0.5 μm (28092-U)
oven: 40 °C (2 min), 50 °C/min to 100 °C, 10 °C/min to 200 °C, 30 °C/min to 325 °C (7.5 min)
inj. temp.: 280 °C, splitless (0.61 min)
detector: MSD, Scan range 45-450 amu, 325°C
carrier gas: helium, pressure programmed, 20 psi (0.0 min), ramp to 80 psi (0.0 min), ramp to 16.5 psi (3 min), ramp to 25 psi (hold for remainder of run)
injection: 1 μL, splitless (0.61 min)
liner: 4 mm I.D., single taper
sample: 50 ng on-column of a 62 Supplemental Appendix IX list consisting of semivolatile standards, 6 internal standards, and 8 surrogates
应用
environmental
法律信息
分析物
说明
Pentachloronitrobenzene
3-Methylcholanthrene
Methyl methanesulfonate
1-Methylnaphthalene
2,4,6-Tribromophenol
7,12-Dimethylbenz[a]anthracene
Diphenylamine
Famphur
Phenacetin
3-Methylphenol, analytical standard
2-Fluorobiphenyl
Chlorobenzilate
Pentachloroethane
Thionazin
o-Toluidine
N-Nitrosodiethylamine
Aniline
1-Naphthylamine
Acetophenone
Hexachloropropene
Parathion
1,3-Dinitrobenzene
Benzyl alcohol
Naphthalene-d8
Safrole
1,4-Dinitrobenzene
Nitrobenzene-d5
Pentachlorobenzene
α,α-Dimethylphenethylamine
Methyl parathion, analytical standard
Kepone
1,3,5-Trinitrobenzene
1,4-Dichlorobenzene-d4
Ethyl methanesulfonate
2-Fluorophenol
5-Nitro-o-toluidine, analytical standard
N-Nitrosopyrrolidine
Perylene-d12
Phenol-d6
1,2-Dichlorobenzene-d4
2,6-Dichlorophenol
2,3,4,6-Tetrachlorophenol
4-Nitroquinoline N-oxide
Dibenz[a,h]acridine
2-Picoline
N-Nitrosomethylethylamine
2-Naphthylamine
1,4-Naphthoquinone
4-Aminobiphenyl
Pyridine
Acenaphthene-d10
Disulfoton
Dinoseb
Phorate
1,2,4,5-Tetrachlorobenzene
1,4-Dioxane
2,3,5,6-Tetrachlorophenol
Dimethoate
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