GC Analysis of Basic Drugs on SLB^®-5ms

技术

gas chromatography (GC): suitable

试验参数

column: SLB-5ms, 30 m x 0.25 mm I.D., 0.50 μm (28473-U)
oven: 45 °C (2.0 min), 30 °C/min to 110 °C (1.0 min), 15 °C/min to 200 °C (1.0 min), 4 °C/min to 310 °C (5.0 min)
inj. temp.: 250 °C
MSD interface: 330 °C
scan range: m/z = 40-450
carrier gas: helium, 0.7 mL/min constant
injection: 0.5 μL, pulsed splitless, 30 psi (0.20 min), purge on (1.50 min), purge flow (50.0 mL/min)
liner: 2 mm I.D., straight
sample: drugs of abuse standard diluted to 100 ppm in methanol

应用

forensics and toxicology