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关键词:'216046'
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Paul D Rainville et al.
Bioanalysis, 4(23), 2833-2842 (2012-12-12)
Accurate mass based LC-MS combined with statistical analysis is established as a core analytical technology for metabonomic studies. This is primarily due to the specificity, sensitivity and structural elucidation capabilities of the technology. The vast majority of these studies are
Hatem A Abdel-Aziz et al.
Molecules (Basel, Switzerland), 18(2), 2084-2095 (2013-02-08)
Although salicylaldehyde azine (3) was reported in 1985 as the single product of the reaction of ethyl 2-oxo-2H-chromene-3-carboxylate (1) with hydrazine hydrate, we identified another main reaction product, besides 3, which was identified as malono-hydrazide (4). In the last
Weidong Qu et al.
Biosensors & bioelectronics, 42, 430-433 (2012-12-19)
Graphene-nickel nanoparticle hybrid was prepared by the one-step far infrared-assisted reduction of graphene oxide and nickel (II) ions using hydrazine. It was loaded on the surface of a magnetic electrode for electrochemical sensing. The feasibility and performance of the novel
Satoshi Watanabe et al.
Journal of oleo science, 62(2), 65-71 (2013-02-09)
We report a useful lithographic technique for the fabrication of organic or metal films on wettability-patterned surfaces fabricated solely through self-assembly. The phase-separated structures in mixed Langmuir-Blodgett (LB) films can be tuned by adjusting intermolecular interactions in film-forming molecules such
Gold nanoparticles formation in the aqueous system of gold (III) chloride complex ions and hydrazine sulfate-kinetic studies.
Streszewski B, et al.
Colloids and Surfaces. A, Physicochemical and Engineering Aspects, 397, 63-72 (2012)
Timothy M Alligrant et al.
Lab on a chip, 13(3), 349-354 (2012-12-06)
We report on real-time electrochemical detection of individual DNA hybridization events at an electrode surface. The experiment is carried out in a microelectrochemical device configured with a working electrode modified with single-stranded DNA probe molecules. When a complementary DNA strand
Tumorigenesis studies with 1,2-dimethylhydrazine dihydrochloride, hydrazine sulfate, and isonicotinic acid in golden hamsters.
B Toth
Cancer research, 32(4), 804-807 (1972-04-01)
Eunhee Lee et al.
Journal of nanoscience and nanotechnology, 12(12), 8886-8892 (2013-03-02)
Pd nanoparticle catalysts supported by thiolated graphene oxide (tGO) on a glassy carbon electrode (GCE), and denoted as tGO-Pd/GCE, are used in this study for the electrochemical determination of hydroxylamine and hydrazine. The physicochemical properties of tGO-Pd were characterized by
Azo Compounds. 1 A Re-examination of the Structure of the Product from the Reaction of Heptane-2, 6-dione with Hydrazine Sulfate and Sodium Cyanide in Dilute Solution.
Overberger CG and Marks BS.
Journal of the American Chemical Society, 77(15), 4097-4100 (1955)
Chirantan Kar et al.
Inorganic chemistry, 52(2), 743-752 (2013-01-11)
We have synthesized a new indole functionalized rhodamine derivative L(1) which specifically binds to Cu(2+) in the presence of large excess of other competing ions with visually observable changes in their electronic and fluorescence spectral behavior. These spectral changes are
Nadia A Mohamed et al.
Molecules (Basel, Switzerland), 17(12), 13969-13988 (2012-11-28)
Twelve novel intrinsically colored wholly aromatic azopolyamide-hydrazides containing various proportions of para- and meta-phenylene units were successfully synthesized by a low temperature (-10 °C) solution polycondensation reaction of either 4-amino-3-hydroxybenzhydrazide (4A3HBH) or 3-amino-4-hydroxybenzhydrazide (3A4HBH) with an equimolar amount of either
Sasanka Dalapati et al.
Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy, 102, 314-318 (2012-12-12)
Test paper coated with Schiff base [(N,N(/)-bis(5-nitro-salicylidene)hydrazine] receptor 1 (host) can selectively detect fluoride and acetate ions (guest) by developing yellow color which can be detected by naked-eye both in aqueous-acetonitrile solution and in solid supported test kit. UV-vis spectral
Proton magnetic resonance spectra of hydrazine salts. Part 1.
Pratt L and Richards RE.
Transactions of the Faraday Society, 49, 744-751 (1953)
Muhammad Baseer et al.
Pakistan journal of pharmaceutical sciences, 26(1), 67-73 (2012-12-25)
Fourteen new N-acetylated and non-acetylated pyrazoline derivatives were synthesized by reacting chalcones with hydrazine in the presence of absolute ethanol however reaction was carried out in the presence of glacial acetic acid to afford N-acetylated pyrazolines. The chemical structures of
John M Keith
The Journal of organic chemistry, 77(24), 11313-11318 (2012-12-12)
Various pyridine, quinoline, isoquinoline, and pyrimidine N-oxides were converted to their corresponding α-N-aryltriflamidoheteroarenes in good yield by treatment with N-aryltriflimides, both neat and in solution, at temperatures ranging from rt to 100 °C.
Erika Lattová et al.
Mass spectrometry reviews, 32(5), 366-385 (2013-01-25)
Over the last years, extensive studies have evaluated glycans from different biological samples and validated the importance of glycosylation as one of the most important post-translational modifications of proteins. Although a number of new methods for carbohydrate analysis have been
Mild and rapid Pd-catalyzed cross-coupling with hydrazine in continuous flow: application to the synthesis of functionalized heterocycles.
Andrew DeAngelis et al.
Angewandte Chemie (International ed. in English), 52(12), 3434-3437 (2013-02-14)
Leslie D Field et al.
Inorganic chemistry, 52(3), 1570-1583 (2013-01-24)
Treatment of [RuCl(PP(3)(iPr))](+)Cl(-) (PP(3)(iPr) = P(CH(2)CH(2)P(i)Pr(2))(3)) with hydrazine, phenylhydrazine, and methylhydrazine afforded side-on bound hydrazine complexes [RuCl(η(2)-H(2)N-NH(2))(η(3)-PP(3)(iPr))](+), [RuCl(η(2)-H(2)N-NHPh)(η(3)-PP(3)(iPr))](+), and [RuCl(η(2)-H(2)N-NHMe)(η(3)-PP(3)(iPr))](+). The analogous reactions of [RuCl(2)(PP(3)(Ph))] (PP(3)(Ph) = P(CH(2)CH(2)PPh(2))(3)) with hydrazine, phenylhydrazine, and methylhydrazine afforded end-on bound hydrazine complexes [RuCl(η(1)-H(2)N-NH(2))(PP(3)(Ph))](+), [RuCl(η(1)-H(2)N-NHPh)(PP(3)(Ph))](+)
Xiuling Yan et al.
Scientific reports, 2, 941-941 (2012-12-12)
Dealloyed nanoporous gold leaves (NPGLs) are found to exhibit high electrocatalytic properties toward both hydrazine (N(2)H(4)) oxidation and hydrogen peroxide (H(2)O(2)) reduction. This observation allows the implementation of a direct hydrazine-hydrogen peroxide fuel cell (DHHPFC) based on these novel porous
Shubin Liu
The journal of physical chemistry. A, 117(5), 962-965 (2013-01-19)
Bond rotations are common and important in molecular studies such as drug design and enzymatic reactions. Steric hindrance and hyperconjugation are often borrowed to justify the origin of bond rotation barriers. However, there exists no consensus, even for as simple
Synthesis and Characterization of Salicylaldazine and Its Metal (II) Complexes Derived from Metal (II) Chlorides.
Wazir J.
International Journal of Medical Works (2016)
Jonas Nilsson et al.
Methods in molecular biology (Clifton, N.J.), 951, 79-100 (2013-01-09)
Extracellular glycoproteins frequently carry terminal sialic acids on their N-linked and/or O-linked glycan structures. In this chapter a sialic acid specific capture-and-release protocol for the enrichment of N- and O-glycopeptides originating from glycoproteins in complex biological samples is described. The
Yinhu Wang et al.
Biosensors & bioelectronics, 43, 180-185 (2013-01-12)
We report a novel hydrogen peroxide (H2O2) and hydrazine sensor based on low-cost poly(vinylpyrrolidone)-protected silver nanocubes (PVP-AgNCs). The monodisperse silver nanocubes were prepared by adding a trace amount of sodium sulfide in the conventional polyol synthesis for fast reduction of
Ranendu Sekhar Das et al.
Dalton transactions (Cambridge, England : 2003), 42(11), 4068-4080 (2013-01-24)
PVP capped platinum nano particles (PNP) of 5 nm diameter were prepared and characterized as homogeneous and of spherical nature. At physiological pH range (6.0-8.0), these PNP catalyze the deoxygenation of phenoxazine group containing resazurin (1) by hydrazine. The observed
J Gold
Nutrition and cancer, 9(2-3), 59-66 (1987-01-01)
Hydrazine sulfate is an anticachexia agent which interrupts host energy wasting as a result of the malignant process. An inhibitor of gluconeogenesis at the phosphoenolpyruvate carboxykinase (PEP CK) reaction, this agent has been shown in randomized, placebo-controlled, double-blind trials to
Alya M Al-Etaibi et al.
Molecules (Basel, Switzerland), 17(12), 13891-13909 (2012-11-28)
A series of new monoazo disperse dyes containing pyrazolopyrimidine moieties was synthesized by coupling malononitrile or 3-aminocrotononitrile with 4-hydroxy- benzenediazonium chloride. Treatment of the resulting products with hydrazine hydrate yields the corresponding 4-arylazoaminopyrazoles, which then react with either 2,4-pentanedione and
Donald A Robinson et al.
ACS nano, 9(7), 7583-7595 (2015-07-15)
An integrated microfluidic/magnetophoretic methodology was developed for improving signal response time and detection limits for the chronoamperometric observation of discrete nanoparticle/electrode interactions by electrocatalytic amplification. The strategy relied on Pt-decorated iron oxide nanoparticles which exhibit both superparamagnetism and electrocatalytic activity
Muhammad Sani Usman et al.
Molecules (Basel, Switzerland), 17(12), 14928-14936 (2012-12-18)
Herein we report a synthesis of copper nanoparticles (Cu-NPs) in chitosan (Cts) media via a chemical reaction method. The nanoparticles were synthesized in an aqueous solution in the presence of Cts as stabilizer and CuSO(4)·5H(2)O precursor. The synthesis proceeded with
Mohammad Mahdi Doroodmand
Materials science & engineering. C, Materials for biological applications, 33(4), 1969-1974 (2013-03-19)
Effect of "Discrete Fourier Transform" (DFT) is studied for electrochemical detection of some electroactive species using multi-walled carbon nanotube/polyacrylonitrile ceramic fiber as ultra micro electrode. Based on DFT theory, two independent phases i.e. the imaginary and real phases are evaluated
Johann Glück et al.
Chemistry (Weinheim an der Bergstrasse, Germany), 20(48), 15947-15960 (2014-10-07)
The investigation of green-burning boron-based compounds as colorants in pyrotechnic formulations as alternative for barium nitrate, which is a hazard to health and to the environment, is reported. Metal-free and nitrogen-rich dihydrobis(5-aminotetrazolyl)borate salts and dihydrobis(1,3,4-triazolyl)borate salts have been synthesized and
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