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Adriano A Mendes et al.
Journal of industrial microbiology & biotechnology, 38(8), 1055-1066 (2010-10-06)
This work aimed at the production of stabilized derivatives of Thermomyces lanuginosus lipase (TLL) by multipoint covalent immobilization of the enzyme on chitosan-based matrices. The resulting biocatalysts were tested for synthesis of biodiesel by ethanolysis of palm oil. Different hydrogels
C Crews et al.
Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment, 30(1), 11-45 (2012-10-02)
Esters of 2 - and 3-monochloropropane-1,2-diol (MCPD) and glycidol esters are important contaminants of processed edible oils used as foods or food ingredients. This review describes the occurrence and analysis of MCPD esters and glycidol esters in vegetable oils and
Synthesis and characterization of amphiphilic chitosan derivatives as a nano-carrier for paclitaxel delivery.
Huofei Zhou et al.
Journal of controlled release : official journal of the Controlled Release Society, 152 Suppl 1, e124-e125 (2011-12-27)
Glycidol.
Report on carcinogens : carcinogen profiles, 12, 215-216 (2011-08-20)
Effect of imprinting sol-gel immobilized lipase with chiral template substrates in esterification of (R)-(+)-and (S)-(-)-glycidol.
Furukawa S, et al.
Journal of Molecular Catalysis. B, Enzymatic, 17(1), 23-28 (2002)
Ryo Tanaka et al.
Bioorganic & medicinal chemistry letters, 21(14), 4180-4182 (2011-06-17)
The efficient synthesis of 3-O-thia-cPAs (4a-d), sulfur analogues of cyclic phosphatidic acid (cPA), has been achieved. The key step of the synthesis is an intramolecular Arbuzov reaction to construct the cyclic thiophosphate moiety. The present synthetic route enables the synthesis
Huofei Zhou et al.
Biomacromolecules, 11(12), 3480-3486 (2010-10-30)
Novel amphiphilic chitosan derivatives (glycidol-chitosan-deoxycholic acid, G-CS-DCA) were synthesized by grafting hydrophobic moieties, deoxycholic acid (DCA), and hydrophilic moieties, glycidol, with the purpose of preparing carriers for poorly soluble drugs. Based on self-assembly, G-CS-DCA can form nanoparticles with size ranging
A practical synthesis of (S)-HPMPC.
Brodfuehrer PR, et al.
Tetrahedron Letters, 35(20), 3243-3246 (1994)
Hiroshi Honda et al.
Food and chemical toxicology : an international journal published for the British Industrial Biological Research Association, 50(11), 4163-4168 (2012-08-15)
Glycidol fatty acid esters (GEs) have been found as impurities in refined edible oils including diacylglycerol (DAG) oil, and concerns of possible exposure to glycidol (G), a known animal carcinogen, during digestion have been raised. We previously measured N-(2,3-dihydroxy-propyl)valine (diHOPrVal)
V Arjunan et al.
Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy, 96, 24-34 (2012-06-02)
The FT-IR and FT-Raman spectra of H bond inner conformer of 2,3-epoxypropanol have been recorded in the regions 3700-400 and 3700-100 cm(-1), respectively. The spectra were interpreted in terms of fundamentals modes, combination and overtone bands. The normal coordinate analysis
A Becalski et al.
Analytical and bioanalytical chemistry, 403(10), 2933-2942 (2012-03-31)
An improved method based on liquid chromatography-tandem mass spectrometry (LC-MS/MS) for the analysis of glycidyl fatty acid esters in oils was developed. The method incorporates stable isotope dilution analysis (SIDA) for quantifying the five target analytes: glycidyl esters of palmitic
Naohiro Ikeda et al.
Food and chemical toxicology : an international journal published for the British Industrial Biological Research Association, 50(11), 3927-3933 (2012-08-28)
Glycidol fatty acid esters (GEs) are found in refined edible oils. Safety concerns have been alleged due to the possible release of glycidol (G), an animal carcinogen. We evaluated the genotoxic potential of glycidol linoleate (GL), a primary GE found
Synthesis of propane-2, 3-diol combinatorial monomers.
Acevedo OL and Andrews RS.
Tetrahedron Letters, 37(23), 3931-3934 (1996)
Rajesh A Shenoi et al.
Biomacromolecules, 13(10), 3018-3030 (2012-08-28)
Herein we report the synthesis of biodegradable hyperbranched polyglycerols (BHPGs) having acid-cleavable core structure by anionic ring-opening multibranching polymerization (ROMBP) of glycidol using initiators bearing dimethyl and cyclohexyl ketal groups. Five different multifunctional initiators carrying one to four ketal groups
Jing Xu et al.
Colloids and surfaces. B, Biointerfaces, 95, 201-207 (2012-03-23)
The effect of aggregation behavior of gelatin in aqueous solution on the grafting density of glycidol grafted gelatin polymers (GGG polymers) was investigated. The grafting density was measured using the Van Slyke method by calculating the conversion rate of free
Koichi Sawada et al.
Journal of bioscience and bioengineering, 114(2), 204-208 (2012-05-19)
Electrospun polyvinyl alcohol (PVA) nanofibrous non-woven fabrics have been widely used for cell and enzyme immobilization. Enhancement of the productivity of the material will further enlarge the versatility of them. In this study, a mixture of water and N,N-dimethylformamide (DMF)
Benjamin R Spears et al.
Chemical communications (Cambridge, England), 49(24), 2394-2396 (2013-02-02)
The control of the branching in polyglycidols as semibranched alternatives to traditional polyglycidols is presented. The relative abundance of dendritic carbons is lowered by five-fold compared to hyperbranched polyglycidols. It is the first example of tailoring the branching in polyglycidol
Hiroshi Honda et al.
Food and chemical toxicology : an international journal published for the British Industrial Biological Research Association, 49(10), 2536-2540 (2011-07-12)
Hemoglobin (Hb) adducts are frequently used to address and/or monitor exposure to reactive chemicals. Glycidol (G), a known animal carcinogen, has been reported to form Hb adducts. Here, we measure G adduct levels in humans who daily ingest DAG oil
Lei Wang et al.
Biotechnology and applied biochemistry, 56(1), 1-6 (2010-04-20)
A novel plasmid (pBSR2) was constructed by incorporating a strong lipase promoter and a terminator into the original pBD64. The lipase gene from Bacillus subtilis strain IFFI10210 was cloned into the plasmid pBSR2 and transformed into B. subtilis A.S.1.1655 to
N Frank et al.
Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment, 30(1), 69-79 (2012-10-23)
Glycidyl esters (GEs) are known to be formed during vegetable oil processing. Because of their structure, it has been hypothesised that GEs, like fatty acid esters of chloropropanols (MCPD esters), may be accepted as substrates by gut lipases to release
B D Craft et al.
Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment, 30(1), 46-51 (2012-10-02)
Recently, fatty acid esters of monochloropropanediol (MCPD) and that of glycidol have been reported in refined edible oils. Since then a wealth of research has been published on the factors influencing the formation of these contaminants in foods. It can
Tetrahedron Letters, 47, 6401-6401 (2006)
Hui Lin et al.
Chemical communications (Cambridge, England), 47(9), 2610-2612 (2011-01-15)
Enantiomerically enriched glycidol derivatives with contiguous stereogenic centers were obtained in a highly diastereo- and enantio-selective epoxidation catalyzed with the styrene monooxygenase StyAB2.
A New Route for Protected Amino Alcohols from (R)-Glycidol. Copper (I) Mediated Alkylation of 4-Tosyloxymethyl-2-oxazolidinone.
Iwama S and Katsumura S.
Bulletin of the Chemical Society of Japan, 67(12), 3363-3365 (1994)
Nadiya Bakhiya et al.
Molecular nutrition & food research, 55(4), 509-521 (2011-02-26)
Fatty acid esters of 3-chloropropane-1,2-diol (3-MCPD) and glycidol are a newly identified class of food process contaminants. They are widespread in refined vegetable oils and fats and have been detected in vegetable fat-containing products, including infant formulas. There are no
Mathieu Dubois et al.
Journal of agricultural and food chemistry, 59(23), 12291-12301 (2011-10-25)
A method based on a gel permeation chromatography (GPC) extraction procedure combined with an additional cleanup by solid-phase extraction (SPE) on silica gel and liquid chromatography-mass spectrometry (LC-MS) detection has been validated for the analysis of seven glycidyl esters (GEs)
Synthesis of amino-1, 4-anhydro-d-pentitols and amino-1, 5-anhydro-d-hexitols with the arabino configuration from (R)-glycidol.
Aragones S, et al.
Tetrahedron Asymmetry, 14(13), 1847-1856 (2003)
Javix Thomas et al.
Chemistry (Weinheim an der Bergstrasse, Germany), 17(16), 4582-4587 (2011-03-25)
Chirality recognition in the hydrogen-bonded glycidol···propylene oxide complex has been studied by using rotational spectroscopy and ab initio calculations. An extensive conformational search has been performed for this binary adduct at the MP2/6-311++G(d,p) level of theory and a total of
Diastereoselective synthesis of ?-hydroxy-?-amino alcohols,(2S, 3S)-and (2S, 3R)-threoninol and-hydroxyphenylalaninol, from (R)-glycidol via the derived 4-hydroxymethyloxazolidinone.
Katsumura S, et al.
Tetrahedron Asymmetry, 5(2), 161-164 (1994)
Troy D Haines et al.
Journal of the American Oil Chemists' Society, 88(1), 1-14 (2011-02-26)
Analysis of MCPD esters and glycidyl esters in vegetable oils using the indirect method proposed by the DGF gave inconsistent results when salting out conditions were varied. Subsequent investigation showed that the method was destroying and reforming MCPD during the
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