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  • [Peculiarities of tetramethyltiuram disulfide detection in the biological material].

[Peculiarities of tetramethyltiuram disulfide detection in the biological material].

Sudebno-meditsinskaia ekspertiza (2010-06-22)
V K Shormanov, A V Kim, E P Duritsyn, Iu N Baranov
摘要

Optimal conditions for the extraction of tetramethyltiuram disulfide (TMTD) from biological materials with ethylacetate are described. The isolated compound can be separated from co-extracted impurities on a silicagel L (40/100 mcm) column. Identification and quantitative determination of TMTD purified from cadaverous liver were performed using thin-layer chromatography, IR spectrophotometry, and high performance liquid chromatography with UF detection.

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Sigma-Aldrich
二硫化四甲基秋兰姆, 97%
Supelco
福美双, PESTANAL®, analytical standard