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  • Iodo-cyclizations: novel strategy for the total syntheses of polyrhacitide A and epi-cryptocaryolone.

Iodo-cyclizations: novel strategy for the total syntheses of polyrhacitide A and epi-cryptocaryolone.

Organic letters (2011-01-11)
Debendra K Mohapatra, Eswar Bhimireddy, P Sivarama Krishnarao, Pragna P Das, J S Yadav
摘要

Highly stereoselective total syntheses of polyrhacitide A and epi-cryptocaryolone have been achieved in 11 steps with high overall yield of 24% and 28%, respectively, following a recently developed strategy for the construction of trans-2,6-disubstituted-3,4-dihydropyrans. In this report, the versatility of iodo-cyclization for the total syntheses of polyrhacitide A and epi-cryptocaryolone is demonstrated.

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Sigma-Aldrich
3,4-二氢-2H-吡喃, 97%