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  • Synthesis and characterization of a narrow size distribution of zinc oxide nanoparticles.

Synthesis and characterization of a narrow size distribution of zinc oxide nanoparticles.

International journal of nanomedicine (2011-07-29)
A Khorsand Zak, R Razali, W H Abd Majid, Majid Darroudi
摘要

Zinc oxide nanoparticles (ZnO-NPs) were synthesized via a solvothermal method in triethanolamine (TEA) media. TEA was utilized as a polymer agent to terminate the growth of ZnO-NPs. The ZnO-NPs were characterized by a number of techniques, including X-ray diffraction analysis, transition electron microscopy, and field emission electron microscopy. The ZnO-NPs prepared by the solvothermal process at 150°C for 18 hours exhibited a hexagonal (wurtzite) structure, with a crystalline size of 33 ± 2 nm, and particle size of 48 ± 7 nm. The results confirm that TEA is a suitable polymer agent to prepare homogenous ZnO-NPs.

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Sigma-Aldrich
三乙醇胺 盐酸盐, BioXtra, ≥99.5% (titration)
Sigma-Aldrich
三乙醇胺, Vetec, reagent grade, 97%