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  • Zirconia-porcelain bonding: effect of multiple firings on microtensile bond strength.

Zirconia-porcelain bonding: effect of multiple firings on microtensile bond strength.

The journal of adhesive dentistry (2013-04-18)
Flávia Z Trindade, Marina Amaral, Renata M Melo, Marco A Bottino, Luiz Felipe Valandro
摘要

To determine the bond strength between zirconia and porcelain with varying numbers of veneer firing cycles. Fifty specimens of zirconia veneered with feldspathic ceramic were submitted to one (1-firing), two (2-firings), three (3-firings), four (4-firings), or five (5-firings) firing cycles to sinter the porcelain. After the respective number of firings, the specimens were embedded into acrylic resin and sectioned into bars with a 1-mm2 cross-sectional area. The microbars were bonded to a special device and attached to a universal testing machine (Emic DL 1000). Microtensile bond strength testing (MTBS) was performed at 0.5 mm/min. The maximum load for fracture was recorded (N) and the microtensile bond strength was calculated in MPa. Data were analyzed using one-way ANOVA and Tukey's test (α = 0.05). The Weibull modulus and characteristic strength was also calculated for each experimental group. Specimens submitted to a single firing cycle presented the lowest bond strength values (14.1 MPa), two firing cycles provided intermediate bond strength values (15 MPa) and the other groups presented equivalently high values (18.1 - 18.4 MPa). The Weibull modulus did not change between the groups. More than three firing cycles of a veneer ceramic provided higher bond strengths between zirconia and the veneering ceramic.

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Sigma-Aldrich
氧化锆(IV), powder, 5 μm, 99% trace metals basis
Sigma-Aldrich
氧化锆(IV), nanopowder, <100 nm particle size (TEM)
Sigma-Aldrich
氧化锆(IV), 99.99% trace metals basis (purity excludes ~2% HfO2)