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Merck
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  • ZnO nanocrystals anchored graphene: in situ solvothermal synthesis and enhanced photocatalytic performance.

ZnO nanocrystals anchored graphene: in situ solvothermal synthesis and enhanced photocatalytic performance.

Journal of nanoscience and nanotechnology (2014-04-18)
Zimin Dong, Jun Zhang, Weiwei Yuan, Dong Xie, Gaohui Du
摘要

ZnO nanocrystals anchored graphene composite (ZnO/G) was synthesized by a facile in situ solvothermal route. The nanocomposite was characterized by X-ray diffraction (XRD), scanning electron spectroscopy (SEM), transmission electron microscopy (TEM) and Raman spectra (RS). The results indicated that the ZnO particles with an average diameter of ca. 12.6 nm were well-dispersed on the surface of the graphene nanosheets. The optical properties were investigated by fluorescence (PL) and UV diffuse reflectance (UV-VIS). It showed that the nanocomposite displayed a fluorescence quenching property. Furthermore, the nanocomposite showed a remarkably enhanced photocatalytic activity to degrade organic pollutants (MB, MO, Rh-B) under visible light irradiation, with a percentage degradation of MB reaching as high as 99.8% in 60 min.

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Sigma-Aldrich
氧化锌, ReagentPlus®, powder, <5 μm particle size, 99.9%
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石墨, powder, <20 μm, synthetic
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氧化锌, puriss. p.a., ACS reagent, ≥99.0% (KT)
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氧化锌, nanopowder, ≤50 nm particle size
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氧化锌, nanopowder, <50 nm particle size (BET), >97%
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氧化锌,分散体, nanoparticles, <100 nm particle size (TEM), ≤40 nm avg. part. size (APS), 20 wt. % in H2O
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氧化锌, puriss., meets analytical specification of Ph. Eur., BP, USP, 99-100.5% (calc. for dried substance)
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石墨, flakes
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石墨, powder, <45 μm, ≥99.99% trace metals basis
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氧化锌, 99.999% trace metals basis
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氧化锌, nanowires, Length 1 um
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石墨, powder, <150 μm, 99.99% trace metals basis
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石墨, rod, L 150 mm, diam. 3 mm, low density, 99.995% trace metals basis
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石墨, rod, L 150 mm, diam. 6 mm, 99.995% trace metals basis
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氧化锌, analytical standard