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143685

3-羟基-4-甲氧基苯甲醛

Name: 3-羟基-4-甲氧基苯甲醛
Brand: ALDRICH

99%

别名:

3-羟基大茴香醛, 异香兰醛

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关于此项目

线性分子式:

HOC₆H₃(OCH₃)CHO

化学文摘社编号:

621-59-0

分子量:

152.15

UNSPSC Code:

12352100

NACRES:

NA.22

PubChem Substance ID:

24848602

EC Number:

210-694-9

Beilstein/REAXYS Number:

1073021

MDL number:

MFCD00003369

Assay:

99%

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属性

Quality Level

200

assay

99%

bp

179 °C/15 mmHg (lit.)

mp

113-115 °C (lit.)

functional group

aldehyde

SMILES string

[H]C(=O)c1ccc(OC)c(O)c1

InChI

1S/C8H8O3/c1-11-8-3-2-6(5-9)4-7(8)10/h2-5,10H,1H3

InChI key

JVTZFYYHCGSXJV-UHFFFAOYSA-N

说明

General description

3-羟基-4-甲氧基苯甲醛与呋喃-2-羧酸酰肼和噻吩-2-羧酸酰肼缩合生成席夫碱。它与 1-氮杂双环 [2.2.2] 辛-3-酮发生缩合反应生成 ( Z )-2-（3-羟基-4-甲氧基亚苄基）-1-氮杂双环 [2.2.2] 辛-3-酮。

Application

在抗癌药物 ( Z )-combretastatin a-4 和 glyitein 合成的两步立体选择性合成中，使用 3-羟基-4-甲氧基苯甲醛作为起始试剂。

存储类别

11 - Combustible Solids

wgk

WGK 3

flash_point_f

>212.0 °F

flash_point_c

> 100 °C

ppe

dust mask type N95 (US), Eyeshields, Gloves

历史批次信息供参考:

分析证书(COA)

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New monomeric cobalt and cadmium complexes with Schiff-bases, namely, N'-[(E)-(3-hydroxy-4-methoxyphenyl)methylidene]furan-2-carbohydrazide (L¹) and N'-[(E)-(3-hydroxy-4-methoxyphenyl)methylidene]thiophene-2-carbohydrazide (L²) are reported. Schiff-base ligands L¹ and L² were derived from condensation of 3-hydroxy-4-methoxybenzaldehyde (iso-vanillin) with furan-2-carboxylic acid hydrazide and thiophene-2-carboxylic acid hydrazide, respectively. Complexes of the

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4-Methoxyresorcinol (3) was synthesized as the precursor for glycitein (6) synthesis by the oxidation of 3-hydroxy-4-methoxybenzaldehyde (1) to the aryl formate with H2O2 and a catalytic amount of SeO2. Glycitein (6) was synthesized by cyclization of 2,4,4'-trihydroxy-5-methoxydeoxybenzoin (5) with N,N-dimethylformamide

(Z)-2-(3-hydroxy-4-methoxybenzylidene)-1-azabicyclo[2.2.2]octan-3-one.

Vijayakumar N Sonar et al.

Acta crystallographica. Section C, Crystal structure communications, 59(Pt 11), o647-o649 (2003-11-08)

Crystals of the title compound, C(15)H(17)NO(3), were obtained from a condensation reaction of 3-hydroxy-4-methoxybenzaldehyde with 1-azabicyclo[2.2.2]octan-3-one and subsequent crystallization of the product from methanol. The title compound, containing a double bond that connects the azabicyclic ring system to the 3-hydroxy-4-methoxybenzylidene

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全球贸易项目编号

货号	GTIN
143685-100G	04061838734990
143685-25G	04061838735003