157554
1-溴-2,4-二甲氧基苯
97%
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关于此项目
线性分子式:
BrC6H3(OCH3)2
化学文摘社编号:
分子量:
217.06
NACRES:
NA.22
PubChem Substance ID:
UNSPSC Code:
12352100
EC Number:
241-717-0
MDL number:
产品名称
1-溴-2,4-二甲氧基苯, 97%
InChI key
NIUZVSQOXJIHBL-UHFFFAOYSA-N
InChI
1S/C8H9BrO2/c1-10-6-3-4-7(9)8(5-6)11-2/h3-5H,1-2H3
SMILES string
COc1ccc(Br)c(OC)c1
assay
97%
form
liquid
refractive index
n20/D 1.572 (lit.)
bp
153-155 °C/18 mmHg (lit.)
mp
25-26 °C (lit.)
density
1.507 g/mL at 25 °C (lit.)
functional group
bromo
Quality Level
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Application
1-Bromo-2,4-dimethoxybenzene was used in the synthesis of 2,3-disubstituted benzo[b]furans. It was also used in the synthesis of dendrimer Si[CH2CH2Si(Me)2-2,4-(MeO)2-C6H3]4.
flash_point_c
113 °C - closed cup
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
存储类别
10 - Combustible liquids
wgk
WGK 3
flash_point_f
235.4 °F - closed cup
ppe
Eyeshields, Gloves, type ABEK (EN14387) respirator filter
Selective lithiation and crystal structures of G1-carbosilane dendrimers with dimethoxybenzene functionalities.
Harder S, et al.
Journal of Organometallic Chemistry, 689(7), 1095-1101 (2004)
Dawei Yue et al.
The Journal of organic chemistry, 70(25), 10292-10296 (2005-12-06)
[reaction: see text] 2,3-Disubstituted benzo[b]furans are readily prepared under very mild reaction conditions by the palladium/copper-catalyzed cross-coupling of various o-iodoanisoles and terminal alkynes, followed by electrophilic cyclization with I2, PhSeCl, or p-O2NC6H4SCl. Aryl- and vinylic-substituted alkynes undergo electrophilic cyclization in
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