213853
α-乙酰氨基肉桂酸
98%
别名:
N-乙酰基脱氢苯丙氨酸
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线性分子式:
C6H5CH=C(NHCOCH3)COOH
化学文摘社编号:
分子量:
205.21
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
EC Number:
226-795-6
Beilstein/REAXYS Number:
1912549
MDL number:
产品名称
α-乙酰氨基肉桂酸, 98%
InChI key
XODAOBAZOQSFDS-YFHOEESVSA-N
InChI
1S/C11H11NO3/c1-8(13)12-10(11(14)15)7-9-5-3-2-4-6-9/h2-7H,1H3,(H,12,13)(H,14,15)/b10-7-
SMILES string
CC(=O)N\C(=C/c1ccccc1)C(O)=O
assay
98%
mp
188-190 °C (lit.)
solubility
methanol: soluble 100 mg/mL, clear, yellow-green
95% ethanol: soluble 5%, clear, yellow
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General description
Asymmeteric hydrogenation of α-acetamidocinnamic acid with chiral rhodium (I) complexes on charcoal has been reported. α-Acetamidocinnamic acid undergoes asymmetric hydrogenation in ionic liquid catalyzed by rhodium complex to yield (S)-phenylalanine.
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2
存储类别
11 - Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
dust mask type N95 (US), Eyeshields, Gloves
Asymmetric hydrogenation of a-acetamidocinnamic acid with chiral rhodium complexes of DIOP and BPPM on charcoal.
Masami I, et al.
Chemical & Pharmaceutical Bulletin, 31(10), 3371-3376 (1983)
Choong Eui Song
Chemical communications (Cambridge, England), 9(9), 1033-1043 (2004-04-30)
Recent developments in the enantioselective chemo- and bio-catalysis in ionic liquids are reviewed. In many cases, the use of ionic liquids provides many advantages over reactions in conventional organic solvents in terms of activity, enantioselectivity, stability and the reusability of
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