242934
碘代乙酸乙酯
98%
别名:
Ethyl 2-iodoacetate, Ethyl monoiodoacetate, Iodoacetic acid ethyl ester
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线性分子式:
ICH2COOC2H5
化学文摘社编号:
分子量:
214.00
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
EC Number:
210-796-3
Beilstein/REAXYS Number:
741934
MDL number:
Assay:
98%
产品名称
碘代乙酸乙酯, 98%
InChI key
MFFXVVHUKRKXCI-UHFFFAOYSA-N
InChI
1S/C4H7IO2/c1-2-7-4(6)3-5/h2-3H2,1H3
SMILES string
CCOC(=O)CI
assay
98%
refractive index
n20/D 1.503 (lit.)
bp
179-180 °C (lit.)
density
1.808 g/mL at 25 °C (lit.)
functional group
ester
iodo
storage temp.
2-8°C
Quality Level
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Application
Ethyl iodoacetate was used in the synthesis of trans-2,3-disubstituted indolines by reacting with 1-azido-2-allylbenzene derivatives via a diastereoselective radical cascade.
General description
Ethyl iodoacetate, also known as iodoacetic acid ethyl ester, serves as an alkylating agent and a radical precursor in organic synthesis. It is also commonly used as a lachrymatory agent.
signalword
Danger
hcodes
Hazard Classifications
Acute Tox. 2 Oral - Eye Dam. 1 - Skin Corr. 1B
存储类别
6.1A - Combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials
wgk
WGK 3
flash_point_f
170.6 °F - closed cup
flash_point_c
77 °C - closed cup
ppe
Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter
法规信息
危险化学品
此项目有
François Brucelle et al.
The Journal of organic chemistry, 78(12), 6245-6252 (2013-06-01)
The preparation of trans-2,3-disubstituted indolines from 1-azido-2-allylbenzene derivatives via a diastereoselective radical cascade using ethyl iodoacetate and triethylborane is described. Further lactamization afforded substituted benzopyrrolizidinones with excellent diastereomeric ratios. The radical cascade/lactamization sequence was efficiently applied to the synthesis of
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