260908
N-溴酞亚胺
95%
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关于此项目
经验公式（希尔记法）:
C8H4BrNO2
化学文摘社编号:
分子量:
226.03
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
EC Number:
219-467-9
Beilstein/REAXYS Number:
131211
MDL number:
Assay:
95%
产品名称
N-溴酞亚胺, 95%
InChI key
MARXMDRWROUXMD-UHFFFAOYSA-N
InChI
1S/C8H4BrNO2/c9-10-7(11)5-3-1-2-4-6(5)8(10)12/h1-4H
SMILES string
BrN1C(=O)c2ccccc2C1=O
assay
95%
mp
194-198 °C (lit.)
functional group
imide
Quality Level
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Application
N-Bromophthalimide has been used:
- as reagent in allylic amination reactions of alkenes
- brominating reagent in enantioselective synthesis of multisubstituted biaryl derivatives by chiral phosphoric acid catalyzed asymmetric bromination
- as a titrant in titrimetric determination of isoniazid in pure form or in tablets
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
存储类别
11 - Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
dust mask type N95 (US), Eyeshields, Gloves
法规信息
新产品
此项目有
V Krishnakumar et al.
Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy, 62(4-5), 918-925 (2005-06-14)
Fourier transform infrared (FT-IR) spectra of phthalimide and N-bromophthalimide have been recorded in the range of 4000-400 cm-1. With the hope of providing more and effective information on the fundamental vibrations, a normal coordinate analysis has been performed on phthalimide
Titrimetric determination of para-aminobenzoic acid using N-bromophthalimide and N-bromosaccharin.
K G Kumar et al.
Journal of pharmaceutical and biomedical analysis, 7(5), 627-631 (1989-01-01)
Feng Chen et al.
Journal of the American Chemical Society, 135(4), 1232-1235 (2013-01-15)
A catalytic asymmetric bromocyclization of trisubstituted olefinic amides that uses a C(2)-symmetric mannitol-derived cyclic selenium catalyst and a stoichiometric amount of N-bromophthalimide is reported. The resulting enantioenriched pyrrolidine products, which contain two stereogenic centers, can undergo rearrangement to yield 2,3-disubstituted
Ying Wei et al.
Organic letters, 15(20), 5186-5189 (2013-10-10)
Allylic amination reactions of alkenes, with an NBP (N-bromophthalimide) or NBS (N-bromosuccinimide)/DBU combination, were developed, in which both internal and external nitrogen nucleophiles can be installed directly. Dual activation of NBS or NBP by DBU leads to more electrophilic bromine
Titrimetric methods for the determination of some sulpha drugs using N-bromophthalimide and N-bromosaccharin.
K G Kumar et al.
The Analyst, 113(9), 1369-1372 (1988-09-01)
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