270245
4-甲氧基氯苄
contains potassium carbonate as stabilizer, 98%
别名:
4-(氯甲基)苯甲醚
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线性分子式:
CH3OC6H4CH2Cl
化学文摘社编号:
分子量:
156.61
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
EC Number:
212-540-6
Beilstein/REAXYS Number:
606667
MDL number:
Assay:
98%
Form:
liquid
InChI key
MOHYOXXOKFQHDC-UHFFFAOYSA-N
InChI
1S/C8H9ClO/c1-10-8-4-2-7(6-9)3-5-8/h2-5H,6H2,1H3
SMILES string
COc1ccc(CCl)cc1
assay
98%
form
liquid
contains
potassium carbonate as stabilizer
bp
117-118 °C/14 mmHg (lit.)
mp
−1 °C (lit.)
density
1.155 g/mL at 25 °C (lit.)
storage temp.
2-8°C
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General description
4-Methoxybenzyl chloride undergoes mild oxidative claevage with ceric ammonium nitrate.
Application
4-Methoxybenzyl chloride was used to benzylate the aniline nitrogen. It was also used in the synthesis of 1-naphthamide and diarymethanes via Suzuki cross-coupling with postassium aryltrifluoroborates.
O/N protecting group reagent which can be mildly oxidatively cleaved, e.g., with ceric ammonium nitrate.
signalword
Danger
hcodes
Hazard Classifications
Skin Corr. 1B
存储类别
8A - Combustible corrosive hazardous materials
wgk
WGK 3
flash_point_f
228.2 °F - closed cup
flash_point_c
109 °C - closed cup
ppe
Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter
法规信息
新产品
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Gary A Molander et al.
The Journal of organic chemistry, 71(24), 9198-9202 (2006-11-18)
[reaction: see text] The palladium-catalyzed cross-coupling of potassium aryltrifluoroborates with benzylic halides occurs in good yield with high functional group tolerance. The increased stability of potassium aryltrifluoroborates compared to other boron coupling partners makes this an effective route to functionalized
Synthesis of a potent (?)-4-(2-hydroxyphenyl) analogue of the acromelic acids by dearomatising cyclisation of a lithiated N-p-methoxybenzyl-4-methoxy-1-naphthamide.
Tetrahedron Letters, 42(20), 3407-3410 (2001)
Thompson AS, et al.
Tetrahedron Letters, 36(49), 8937-8940 (1995)
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