333549
3-溴环己烯
technical grade, 90%
别名:
2-环己烯-1-基溴
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关于此项目
经验公式（希尔记法）:
C6H9Br
化学文摘社编号:
分子量:
161.04
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
MDL number:
Beilstein/REAXYS Number:
635953
Assay:
90%
Form:
liquid
产品名称
3-溴环己烯, technical grade, 90%
InChI
1S/C6H9Br/c7-6-4-2-1-3-5-6/h2,4,6H,1,3,5H2
SMILES string
BrC1CCCC=C1
InChI key
AJKDUJRRWLQXHM-UHFFFAOYSA-N
grade
technical grade
assay
90%
form
liquid
refractive index
n20/D 1.528 (lit.)
bp
57-58 °C/12 mmHg (lit.)
density
1.4 g/mL at 25 °C (lit.)
functional group
bromo
storage temp.
−20°C
Quality Level
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Application
3-溴环己烯可用于合成 N-叔-丁氧羰基-O-环己基-L-酪氨酸。 它也可用于合成对映纯的环己糖醇，例如 muco-槲皮醇,D-手性-肌醇和 allo-肌醇。
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
存储类别
3 - Flammable liquids
wgk
WGK 3
flash_point_f
129.2 °F - closed cup
flash_point_c
54 °C - closed cup
ppe
Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
危险化学品
此项目有
Synthesis of enantiopure cyclitols from (?)-3-bromocyclohexene mediated by intramolecular oxyselenenylation employing (S, S)-hydrobenzoin and (S)-mandelic acid as chiral sources.
Lee YJ, et al.
Tetrahedron, 61(8), 1987-2001 (2005)
Y Nishiyama et al.
Chemical & pharmaceutical bulletin, 49(2), 233-235 (2001-02-24)
A facile and efficient synthesis of N-tert-butoxycarbonyl-O-cyclohexyl-L-tyrosine [Boc-Tyr(Chx)-OH] is described. Boc-Tyr-OH was treated with NaH in dimethylformamide and then with 3-bromocyclohexene to give N-Boc-O-(cyclohex-2-enyl)-L-tyrosine [Boc-Tyr(Che)-OH] in 70% yield. Hydrogenation of Boc-Tyr(Che)-OH over PtO2 afforded Boc-Tyr(Chx)-OH in almost quantitative yield. The
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