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926728

PMPBO

Name: PMPBO
Brand: ALDRICH

≥95%, powder

别名:

N-Benzyl-N-(5-methyl-[1,1′-biphenyl]-2-yl)oxalamide

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关于此项目

经验公式（希尔记法）:

C₂₂H₂₀N₂O₂

化学文摘社编号:

1909333-82-9

分子量:

344.41

UNSPSC Code:

12352101

NACRES:

NA.21

MDL number:

MFCD30491291

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属性

产品名称

PMPBO, ≥95%

Quality Level

100

assay

≥95%

form

powder

reaction suitability

reagent type: ligand
reaction type: Ullmann Reaction

mp

154-155 °C

storage temp.

−20°C

SMILES string

O=C(C(NCC1=CC=CC=C1)=O)NC2=CC=C(C)C=C2C3=CC=CC=C3

InChI

1S/C22H20N2O2/c1-16-12-13-20(19(14-16)18-10-6-3-7-11-18)24-22(26)21(25)23-15-17-8-4-2-5-9-17/h2-14H,15H2,1H3,(H,23,25)(H,24,26)

InChI key

AWTLXLDETPWZRB-UHFFFAOYSA-N

说明

Application

PMPBO is a ligand for the copper-catalyzed Ullman-Ma cross-coupling reaction.

Other Notes

Copper-Catalyzed Diaryl Ether Formation from (Hetero)aryl Halides at Low Catalytic Loadings

存储类别

11 - Combustible Solids

wgk

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable

法规信息

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分析证书(COA)

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Copper-Catalyzed Diaryl Ether Formation from (Hetero)aryl Halides at Low Catalytic Loadings.

Yuntong Zhai et al.

The Journal of organic chemistry, 82(9), 4964-4969 (2017-04-22)

Diaryl formation is achieved by coupling phenols and (hetero)aryl halides under the catalysis of CuI/N,N'-bis(2-phenylphenyl) oxalamide (BPPO) or CuI/N-(2-phenylphenyl)-N'-benzyl oxalamide (PPBO) at 90 °C using DMF or MeCN as the solvent. Only 0.2-2 mol % CuI and ligand are required

全球贸易项目编号

货号	GTIN
926728-250MG	04065267988092
926728-1G	04065267988085