71478
Nα-（2,4-二硝基-5-氟苯基）-L氨基丙酰胺
derivatization grade (chiral), LiChropur™, ≥99.0%
别名:
FDAA, Marfey 试剂
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关于此项目
经验公式（希尔记法）:
C9H9FN4O5
CAS Number:
分子量:
272.19
Beilstein:
6820069
MDL编号:
UNSPSC代码:
23151816
PubChem化学物质编号:
NACRES:
NA.22
等级
derivatization grade (chiral)
质量水平
方案
≥99.0% (sum of enantiomers, TLC)
≥99.0%
表单
powder
旋光性
[α]20/D +56±2°, c = 1% in acetone
光学纯度
enantiomeric ratio: ≥99.5:0.5 (HPLC)
质量
LiChropur™
技术
HPLC: suitable
储存温度
2-8°C
SMILES字符串
C[C@H](Nc1cc(F)c(cc1[N+]([O-])=O)[N+]([O-])=O)C(N)=O
InChI
1S/C9H9FN4O5/c1-4(9(11)15)12-6-2-5(10)7(13(16)17)3-8(6)14(18)19/h2-4,12H,1H3,(H2,11,15)/t4-/m0/s1
InChI key
NEPLBHLFDJOJGP-BYPYZUCNSA-N
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Warning
危险声明
危险分类
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
靶器官
Respiratory system
储存分类代码
11 - Combustible Solids
WGK
WGK 3
闪点(°F)
Not applicable
闪点(°C)
Not applicable
个人防护装备
dust mask type N95 (US), Eyeshields, Gloves
Chirality determination of unusual amino acids using precolumn derivatization and liquid chromatography-electrospray ionization mass spectrometry.
Hess S
Journal of Chromatography A, 1035(2), 211-219 (2004)
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Marine natural products are important resources for discovering novel anticancer drugs. In this study, an extract prepared from the culture of a sea anemone-derived actinomycete Streptomyces sp. ZZ406 in soluble starch and casein-related liquid medium was found to have activity
B S Foster et al.
Journal of analytical toxicology, 22(4), 265-269 (1998-07-29)
An analytical method was developed for enantiomeric determination of amphetamine and methamphetamine in human urine. The enantiomers were isolated from urine by solid-phase extraction, and diastereomers were formed by derivatization with the chiral Marfey's reagent (1-fluoro-2,4-dinitrophenyl-5-l-aniline amide). The diastereomers were
E Harth-Fritschy et al.
The journal of peptide research : official journal of the American Peptide Society, 50(6), 415-420 (1998-01-24)
Esterification of glycosylated serine and cysteine derivatives with a 4-alkoxybenzyl alcohol (Wang) resin is described. The classical methods of ester bond formation (symmetrical anhydride, 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium tetrafluoroborate [TBTU]/4-dimethylaminopyridine [DMAP] with or without 1-hydroxybenzotriazole [HOBT], pentafluorophenyl [Pfp] esters gave high percentages of
R Bhushan et al.
Amino acids, 27(3-4), 231-247 (2004-10-27)
The present paper describes characteristics and application of Marfey's reagent (MR) including general protocols for synthesis of the reagent and diastereomers along with advantages, disadvantages and the required precautions. Applications, and comparison with other derivatizing agents, for the resolution of
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