Merck
CN
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文件

安全信息

571261

Sigma-Aldrich

哌啶

biotech. grade, ≥99.5%

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别名:
六氢吡啶
经验公式（希尔记法）:
C5H11N
CAS号:
110-89-4
分子量:
85.15
Beilstein:
102438
EC 号:
203-813-0
MDL编号:
MFCD00005979
PubChem化学物质编号:
329758271
NACRES:
NA.21

等级

biotech. grade

质量水平

100

蒸汽密度

3 (vs air)

蒸汽压

23 mmHg ( 20 °C)

检测方案

≥99.5%

形式

liquid

technique(s)

DNA sequencing: suitable

杂质

<0.3% water

折射率

n20/D 1.452 (lit.)

bp

106 °C (lit.)
106 °C

mp

−13 °C (lit.)

溶解性

organic solvents: soluble(lit.)
water: miscible(lit.)

密度

0.862 g/mL at 20 °C (lit.)

λ

1 cm path, H2O reference

紫外吸收

λ: 290 Amax: <1.000
λ: 370 Amax: <0.050

SMILES string

C1CCNCC1

InChI

1S/C5H11N/c1-2-4-6-5-3-1/h6H,1-5H2

InChI key

NQRYJNQNLNOLGT-UHFFFAOYSA-N

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相关类别

一般描述

Piperidine, a heterocyclic cyclohexane is a volatile secondary amine. Maxam-Gilbert chemical method, a DNA sequencing technology employs piperidine to rupture DNA strands at damaged base site. Its crystal structure analyzed at 150K shows hydrogen bonding between NH groups. Piperidine ring forms a part of many naturally occuring alkaloids. It is prepared on an industrial scale by the hydrogenation of pyridine in the presence of nickel catalyst. The 1H NMR spectrum of piperidine has been recorded.

应用

适用于 Applied Biosystems 431 和 433A 多肽合成仪。
Piperidine has been used in combination with DMF (dimethylformamide) for the removal of Fmoc (fluorenylmethyloxycarbonyl) group from the N-terminal amino group during peptide synthesis.

警示用语：

Danger

危险分类

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 4 Oral - Eye Dam. 1 - Flam. Liq. 2 - Skin Corr. 1B

储存分类代码

3 - Flammable liquids

WGK

WGK 1

闪点(°F)

60.8 °F - closed cup

闪点(°C)

16 °C - closed cup

法规信息

易制毒化学品（2类）
危险化学品

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Peptide Synthesis.
Miao Z and Cheng Z
Bio-protocol, 2(14) (2012)
W B Mattes et al.
Biochimica et biophysica acta, 868(1), 71-76 (1986-10-16)
The volatile, secondary amine piperidine is used in the Maxam-Gilbert chemical method of DNA sequencing to create strand breaks in DNA at sites of damaged bases. As such it is often used in generalized studies of DNA damage to identify
Andrew Parkin et al.
Acta crystallographica. Section B, Structural science, 60(Pt 2), 219-227 (2004-03-16)
The crystal structures of piperazine, piperidine and morpholine have been determined at 150 K. All three structures are characterized by the formation of NH...N hydrogen-bonded chains. In piperazine these are linked to form sheets, but the chains are shifted so
Total synthesis of (-)-kopsinine by an asymmetric one-pot [n+2+3] cyclization.
Shingo Harada et al.
Chemistry, an Asian journal, 7(10), 2196-2198 (2012-08-22)
Xuwang Chen et al.
Bioorganic & medicinal chemistry, 20(12), 3856-3864 (2012-05-18)
A novel series of piperidine-linked amino-triazine derivatives were designed, synthesized and evaluated for in vitro anti-HIV activity as non-nucleoside reverse transcriptase inhibitors on the basis of our previous work. Screening results indicated that most compounds showed excellent activity against wild-type
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